Kraft P, Bergamaschi A, Broennimann Ch, Dinapoli R, Eikenberry E F, Henrich B, Johnson I, Mozzanica A, Schlepütz C M, Willmott P R, Schmitt B
Paul Scherrer Institut, CH-5232 Villigen PSI, Switzerland.
J Synchrotron Radiat. 2009 May;16(Pt 3):368-75. doi: 10.1107/S0909049509009911. Epub 2009 Apr 7.
PILATUS is a silicon hybrid pixel detector system, operating in single-photon-counting mode, that has been developed at the Paul Scherrer Institut for the needs of macromolecular crystallography at the Swiss Light Source (SLS). A calibrated PILATUS module has been characterized with monochromatic synchrotron radiation. The influence of charge sharing on the count rate and the overall energy resolution of the detector were investigated. The dead-time of the system was determined using the attenuated direct synchrotron beam. A single module detector was also tested in surface diffraction experiments at the SLS, whereby its performance regarding fluorescence suppression and saturation tolerance were evaluated, and have shown to greatly improve the sensitivity, reliability and speed of surface diffraction data acquisition.
PILATUS是一种硅混合像素探测器系统,工作在单光子计数模式,由保罗·谢尔研究所为瑞士光源(SLS)的大分子晶体学需求而开发。一个经过校准的PILATUS模块已通过单色同步辐射进行了表征。研究了电荷共享对探测器计数率和整体能量分辨率的影响。使用衰减的直接同步辐射束确定了系统的死时间。一个单模块探测器也在SLS的表面衍射实验中进行了测试,评估了其在荧光抑制和饱和耐受性方面的性能,结果表明该探测器极大地提高了表面衍射数据采集的灵敏度、可靠性和速度。