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使用CITIUS电荷积分探测器的布拉格相干衍射成像。

Bragg coherent diffraction imaging with the CITIUS charge-integrating detector.

作者信息

Grimes Michael, Pauwels Kristof, Schülli Tobias U, Martin Thierry, Fajardo Pablo, Douissard Paul-Antoine, Kocsis Menyhert, Nishino Haruki, Ozaki Kyosuke, Honjo Yoshiaki, Nishiyama Hiraki Toshiyuki, Joti Yasumasa, Hatsui Takaki, Levi Mor, Rabkin Eugen, Leake Steven J, Richard Marie-Ingrid

机构信息

Université Grenoble Alpes, CEA Grenoble, IRIG, MEM, NRS, 17 rue des Martyrs, F-38000 Grenoble, France.

ESRF - The European Synchrotron, 71 avenue des Martyrs, F-38000 Grenoble, France.

出版信息

J Appl Crystallogr. 2023 Jun 12;56(Pt 4):1032-1037. doi: 10.1107/S1600576723004314. eCollection 2023 Aug 1.

Abstract

The CITIUS detector is a next-generation high-speed X-ray imaging detector. It has integrating-type pixels and is designed to show a consistent linear response at a frame rate of 17.4 kHz, which results in a saturation count rate of over 30 Mcps pixel when operating at an acquisition duty cycle close to 100%, and up to 20 times higher with special extended acquisition modes. Here, its application for Bragg coherent diffraction imaging is demonstrated by taking advantage of the fourth-generation Extremely Brilliant Source of the European Synchrotron (ESRF-EBS, Grenoble, France). The CITIUS detector outperformed a photon-counting detector, similar spatial resolution being achieved (20 ± 6 nm versus 22 ± 9 nm) with greatly reduced acquisition times (23 s versus 200 s). It is also shown how the CITIUS detector can be expected to perform during dynamic Bragg coherent diffraction imaging measurements. Finally, the current limitations of the CITIUS detector and further optimizations for coherent imaging techniques are discussed.

摘要

CITIUS探测器是一款下一代高速X射线成像探测器。它具有积分型像素,设计用于在17.4 kHz的帧率下呈现一致的线性响应,这使得在采集占空比接近100%时,饱和计数率超过30 Mcps/像素,在特殊的扩展采集模式下可达20倍以上。在此,利用欧洲同步辐射装置(ESRF-EBS,法国格勒诺布尔)的第四代极亮光源展示了其在布拉格相干衍射成像中的应用。CITIUS探测器性能优于光子计数探测器,在空间分辨率相近的情况下(分别为20 ± 6 nm和22 ± 9 nm),采集时间大幅缩短(分别为23秒和200秒)。文中还展示了CITIUS探测器在动态布拉格相干衍射成像测量中的预期表现。最后,讨论了CITIUS探测器目前的局限性以及对相干成像技术的进一步优化。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/e955/10405578/df599497d04e/j-56-01032-fig1.jpg

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