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聚酸改性复合树脂(“复合体”)与含氟水溶液的相互作用。

The interaction of polyacid-modified composite resins ('compomers') with aqueous fluoride solutions.

作者信息

Rohani Reza, Nicholson John W

机构信息

School of Science, University of Greenwich, Chatham, United Kingdom.

出版信息

J Appl Oral Sci. 2009 May-Jun;17(3):216-9. doi: 10.1590/s1678-77572009000300016.

Abstract

OBJECTIVE

The aim of this study was to investigate how the release of fluoride from two compomers and a fluoridated composite resin was affected by exposure to KF solution.

MATERIAL AND METHODS

Two compomers (Dyract AP and Compoglass F) and one fluoridated composite (Wave) were prepared as discs (6 mm diameter and 2 mm thick), curing with a standard dental lamp. They were then stored in either water or 0.5% KF for 1 week, followed by placement in water for periods of 1 week up to 5 weeks total. Fluoride was determined with and without TISAB (to allow complexed and decomplexed fluoride to be determined), and other ion release (Na, Ca, Al, Si, P) was determined by ICP-OES.

RESULTS

Specimens were found not to take up fluoride from 100 ppm KF solution in 24 h, but to release additional fluoride when stored for up to five weeks. Compomers released more fluoride cumulatively following exposure to KF solution (p<0.001), all of which was decomplexed, though initial (1 week) values were not statistically significant for Dyract AP. Other ions showed no variations in release over 1 week, regardless of whether the specimens were exposed to KF. Unlike the compomers, Wave showed no change in fluoride release as a result of exposure to KF.

CONCLUSIONS

Compomers are affected by KF solution, and release more fluoride (but not other ions) after exposure than if stored in water.

摘要

目的

本研究旨在调查两种复合体和一种含氟复合树脂在接触氟化钾(KF)溶液时氟的释放情况受到怎样的影响。

材料与方法

将两种复合体(Dyract AP和Compoglass F)以及一种含氟复合材料(Wave)制成圆盘状(直径6毫米,厚2毫米),用标准牙科灯固化。然后将它们分别储存在水中或0.5%的KF溶液中1周,之后再置于水中1周至总共5周。分别在有和没有总离子强度调节缓冲剂(TISAB,用于测定络合和未络合的氟)的情况下测定氟含量,通过电感耦合等离子体发射光谱法(ICP - OES)测定其他离子(钠、钙、铝、硅、磷)的释放量。

结果

发现样本在24小时内不会从100 ppm的KF溶液中摄取氟,但在储存长达5周时会释放额外的氟。复合体在接触KF溶液后累积释放的氟更多(p<0.001),所有释放的氟都是未络合的,尽管Dyract AP最初(1周)的值在统计学上不显著。无论样本是否接触KF,其他离子在1周内的释放量均无变化。与复合体不同,Wave在接触KF后氟释放量没有变化。

结论

复合体受KF溶液影响,接触后比储存在水中释放更多的氟(但其他离子无变化)。

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