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用于生成金属和金属氧化物纳米颗粒测试气溶胶的液体火焰喷雾。

Liquid flame spray for generating metal and metal oxide nanoparticle test aerosol.

作者信息

Mäkelä J M, Aromaa M, Rostedt A, Krinke T J, Janka K, Marjamäki M, Keskinen J

机构信息

Aerosol Physics Laboratory, Tampere University of Technology, Tampere, Finland.

出版信息

Hum Exp Toxicol. 2009 Jun;28(6-7):421-31. doi: 10.1177/0960327109105154.

Abstract

A flame-based method for generating nanoparticles with production rate in the order of g/min is presented to be used in a variety of applied studies concerning nanoparticle measurements and toxicological tests. In this study, ferric oxide, titanium dioxide, and silver nanoparticles were produced by this technique, as an example of the variety of producible compounds, and number and surface area were measured by state-of-art aerosol instruments. In the primary experiments of this study, the generator was used in a conventional way, in a fume cupboard, and the aerosol was measured from the exhaust duct of the cupboard. It has been shown that this steady, turbulent flame generator is also suitable for producing high-concentration aerosols in a wider concept. The generated aerosol was measured by variety of aerosol instrumentation to show the applicability of the generator. When using the generator intentionally as a source of aerosol in the flame processing room, mean nanoparticle sizes of 5-60 nm and active surface area concentration ranges of 1-10,000 microm(2)/cm(3) were covered for the room aerosol.

摘要

本文提出了一种基于火焰的纳米颗粒生成方法,其生产率可达克/分钟量级,可用于各种有关纳米颗粒测量和毒理学测试的应用研究。在本研究中,作为可生产化合物种类的一个示例,通过该技术制备了氧化铁、二氧化钛和银纳米颗粒,并使用先进的气溶胶仪器测量了颗粒数量和表面积。在本研究的初步实验中,发生器以常规方式在通风橱中使用,从通风橱的排气管测量气溶胶。结果表明,这种稳定的湍流火焰发生器在更广泛的概念中也适用于产生高浓度气溶胶。通过各种气溶胶仪器对生成的气溶胶进行测量,以展示该发生器的适用性。当在火焰处理室中有意将该发生器用作气溶胶源时,室内气溶胶的纳米颗粒平均尺寸范围为5 - 60纳米,活性表面积浓度范围为1 - 10000平方微米/立方厘米。

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