Schultz Sabine, Rosentritt Martin, Behr Michael, Handel Gerhard
Department of Prosthetic Dentistry, University of Regensburg, Germany.
Quintessence Int. 2010 Jan;41(1):e1-10.
To compare wear performance and resistance to crack propagation (K1C) of commercial restorative materials and their flowable variations. A potential correlation between three-body wear and fracture toughness, modulus of elasticity, fracture work, Vickers hardness, and filler content was investigated.
Seven restoratives (five composites, one ormocer, and one compomer) and their corresponding flowable materials were used to determine and compare the three-body wear with a bolus of millet-seed shells and rice food (Willytec). The wear characteristics were measured by profilometry after 50,000, 100,000, 150,000, and 200,000 loading cycles. The fracture toughness value, K1C (MPam1/2), for each single-edged notched specimen was measured in a three-point bending test (universal testing machine 1446, Zwick). Fracture work and modulus of elasticity were calculated from the load curves. Vickers hardness was measured (HV hardness tester, Zwick) according to DIN 50133. The veneering composite Sinfony (3M ESPE) was used as a reference material.
Heavily filled composites experienced less wear than their flowable variations. The nanofiller composites revealed better wear results than hybrid composites, compomers, and ormocers. After 200,000 load cycles, the lowest wear rates were detected for Grandio (14 microm; Voco), and the highest mean values were found for Dyract AP (104 microm; Dentsply DeTrey). The values for fracture toughness (K1C) ranged from 0.82 to 3.64 MPam1/2. Highest K1C data was exhibited by the nanocomposite Nanopaq (Schutz Dental). All tested restorative materials exhibited higher fracture toughness than their low-viscosity variations.
The wear resistance of the newer generation composites with incorporated nanofiller or microfiller particles increased to a high extent. Flowables show less resistance against wear and crack propagation because of their lower filler content. The reduced mechanical properties limit their use as a restorative to small noncontact, low-stress clinical situations.
比较市售修复材料及其可流动变体的磨损性能和抗裂纹扩展能力(K1C)。研究三体磨损与断裂韧性、弹性模量、断裂功、维氏硬度和填料含量之间的潜在相关性。
使用七种修复材料(五种复合材料、一种有机陶瓷和一种复合体)及其相应的可流动材料,用一团小米壳和米饭(Willytec)来测定和比较三体磨损。在50000、100000、150000和200000次加载循环后,通过轮廓仪测量磨损特性。在三点弯曲试验(Zwick万能试验机1446)中测量每个单边缺口试样的断裂韧性值K1C(MPam1/2)。根据载荷曲线计算断裂功和弹性模量。按照DIN 50133测量维氏硬度(Zwick HV硬度测试仪)。使用贴面复合材料Sinfony(3M ESPE)作为参考材料。
高填料含量的复合材料比其可流动变体的磨损更少。纳米填料复合材料的磨损结果优于混合复合材料、复合体和有机陶瓷。在200000次加载循环后,Grandio(14微米;Voco)的磨损率最低,Dyract AP(104微米;登士柏德特雷)的平均值最高。断裂韧性(K1C)值范围为0.82至3.64 MPam1/2。纳米复合材料Nanopaq(舒茨牙科)的K1C数据最高。所有测试的修复材料的断裂韧性均高于其低粘度变体。
新一代含有纳米填料或微填料颗粒的复合材料的耐磨性有很大提高。可流动材料由于填料含量较低,显示出较低的耐磨性和抗裂纹扩展能力。力学性能的降低限制了它们在小面积非接触、低应力临床情况下作为修复材料的应用。