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高填充流动性树脂复合材料的弯曲性能、耐磨性及微观结构分析。

Flexural Properties, Wear Resistance, and Microstructural Analysis of Highly Filled Flowable Resin Composites.

机构信息

Philippe Francois, DDS, Faculty of Dental Surgery, Innovative Dental Materials and Interfaces Research Unit (URB2i), Paris Cité University; Bretonneau Hospital, Paris, France.

Jean-Pierre Attal, DDS, PhD, Faculty of Dental Surgery, Innovative Dental Materials and Interfaces Research Unit (URB2i), Paris Cité University; Charles Foix Hospital, Ivry-sur-Seine, France.

出版信息

Oper Dent. 2024 Sep 1;49(5):597-607. doi: 10.2341/24-033-L.

Abstract

OBJECTIVE

This study aimed to evaluate the flexural properties and two-body wear resistance of nine highly filled flowable resin composites relative to those of viscous and conventional low-filled flowable composites. In addition, scanning electron microscopy (SEM) analysis of the microstructures was performed.

METHODS AND MATERIALS

For each resin composite group (n=12), 12 specimen bars (25 mm × 2 mm × 2 mm) were fabricated using a silicon mold for performing flexural strength (FS), flexural modulus (E), flexural toughness (FT), Weibull modulus (m) tests, and SEM microstructural analysis. For each group, ten bars were tested using a three-point flexural test on a universal testing machine, while the other two were embedded in acrylic resin before being observed by SEM for structural analysis. During the two-body wear test with a chewing simulator, 8 specimens (12 groups, n=8) of each resin composite group were manufactured in a specific mold and subjected to 120,000 cycles of wear against a steatite ball, and the depth loss was measured. Three one-way ANOVA tests followed by Tukey's post hoc tests were conducted to compare the flexural and wear properties among the different groups.

RESULTS

The majority of highly filled composites tested in this study exhibited similar flexural strengths (between 105.68 MPa and 135.49 MPa) and superior wear resistance to those of viscous composites. The flexural moduli (between 5.12 GPa and 9.62 GPa) of these composites were in between those of the viscous and low-filled composites tested in this study.

CONCLUSIONS

The highly filled flowable composites tested in this study exhibited different in vitro properties but were often superior to those of viscous resin composite suggesting their possible use for posterior restorations.

摘要

目的

本研究旨在评估 9 种高填充型流动树脂复合材料的弯曲性能和耐两体磨耗性能,并与粘性树脂复合材料和传统低填充型流动树脂复合材料进行比较。此外,还对微观结构进行了扫描电子显微镜(SEM)分析。

方法和材料

对于每种树脂复合材料组(n=12),使用硅模具制作 12 个试件条(25mm×2mm×2mm),以进行弯曲强度(FS)、弯曲模量(E)、弯曲韧性(FT)、韦布尔模量(m)测试和 SEM 微观结构分析。对于每组中的 10 个试件条,在万能试验机上进行三点弯曲试验进行测试,而另外 2 个试件条在被 SEM 观察前嵌入丙烯酸树脂中进行结构分析。在咀嚼模拟器的两体磨耗试验中,每组 8 个试件(n=8)的每种树脂复合材料在特定模具中制造,并与滑石球进行 120000 次磨损循环,测量深度损失。进行了三次单向方差分析(ANOVA)检验,然后进行 Tukey 事后检验,以比较不同组之间的弯曲性能和磨损性能。

结果

本研究中测试的大多数高填充复合材料表现出相似的弯曲强度(在 105.68MPa 和 135.49MPa 之间)和优异的耐磨损性能,优于粘性复合材料。这些复合材料的弯曲模量(在 5.12GPa 和 9.62GPa 之间)介于本研究中测试的粘性和低填充复合材料之间。

结论

本研究中测试的高填充流动复合材料表现出不同的体外性能,但通常优于粘性树脂复合材料,表明它们可能用于后牙修复。

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