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次氯酸钠溶液消毒后微波聚合丙烯酸树脂的物理和机械性能比较

Comparison of physical and mechanical properties of microwave-polymerized acrylic resin after disinfection in sodium hypochlorite solutions.

作者信息

Paranhos Helena de Freitas Oliveira, Davi Letícia Resende, Peracini Amanda, Soares Rafael Bellini, Lovato Cláudia Helena da Silva, Souza Raphael Freitas de

机构信息

Department of Dental Materials and Prosthodontics, Dental School of Ribeirão Preto, University of São Paulo, Ribeirão Preto, SP, Brazil.

出版信息

Braz Dent J. 2009;20(4):331-5. doi: 10.1590/s0103-64402009000400012.

Abstract

This study evaluated the color stability, surface roughness and flexural strength of a microwave-polymerized acrylic resin after immersion in sodium hypochlorite (NaOCl), simulating 20 min of disinfection daily during 180 days. Forty disk-shaped (15 x 4 mm) and 40 rectangular (65 x 10 x 3 mm) specimens were prepared with a microwave-polymerized acrylic resin (Onda-Cryl). Specimens were immersed in either 0.5% NaOCl, 1% NaOCl, Clorox/Calgon and distilled water (control). Color measurements were determined by a portable colorimeter. Three parallel lines, separated by 1.0 mm, were registered on each specimen before and after immersion procedures to analyze the surface roughness. The flexural strength was measured using a 3-point bending test in a universal testing machine with a 50 kgf load cell and a crosshead speed of 1 mm/min. Data were analyzed statistically by ANOVA and Tukey's test (alpha=0.05). There was no statistically significant differences (p>0.05) among the solutions for color, surface roughness and flexural strength. It may be concluded that immersion in NaOCl solutions simulating short-term daily use during 180 days did not influence the color stability, surface roughness and flexural strength of a microwave-polymerized acrylic resin.

摘要

本研究评估了一种微波聚合丙烯酸树脂在次氯酸钠(NaOCl)中浸泡后的颜色稳定性、表面粗糙度和弯曲强度,模拟180天内每天20分钟的消毒过程。用微波聚合丙烯酸树脂(Onda-Cryl)制备了40个圆盘形(15×4毫米)和40个矩形(65×10×3毫米)试样。将试样浸泡在0.5% NaOCl、1% NaOCl、高乐氏/卡尔冈清洁剂和蒸馏水中(对照)。通过便携式色度计测定颜色测量值。在浸泡程序前后,在每个试样上记录三条间距为1.0毫米的平行线,以分析表面粗糙度。使用万能试验机进行三点弯曲试验测量弯曲强度,该试验机配有50千克力的测力传感器,横梁速度为1毫米/分钟。数据采用方差分析和Tukey检验进行统计学分析(α = 0.05)。在颜色、表面粗糙度和弯曲强度方面,各溶液之间无统计学显著差异(p>0.05)。可以得出结论,在模拟180天短期每日使用的情况下,浸泡在NaOCl溶液中不会影响微波聚合丙烯酸树脂的颜色稳定性、表面粗糙度和弯曲强度。

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