Paranhos Helena de Freitas Oliveira, Peracini Amanda, Pisani Marina Xavier, Oliveira Viviane de Cássia, de Souza Raphael Freitas, Silva-Lovato Cláudia Helena
Department of Dental Materials and Prosthodontics, Ribeirão Preto Dental School, USP - University of São Paulo, Ribeirão Preto, SP, Brazil.
Braz Dent J. 2013;24(2):152-6. doi: 10.1590/0103-6440201302151.
This study evaluated color stability, surface roughness and flexural strength of acrylic resin specimens after immersion in alkaline peroxide and alkaline hypochlorite, simulating a period of one and a half year of use of overnight immersion. Sixty disc-shaped (16x4 mm) and 80 rectangular specimens (65x10x3.3 mm) were prepared from heat-polymerized acrylic resin (Lucitone 550) and distributed into 4 groups (n=20): C1: without immersion, C2: 8 h immersion in distilled water; AP: 8 h immersion in alkaline peroxide effervescent tablet; SH: 8 h immersion in 0.5% NaOCl solution. Properties were evaluated at baseline and after the immersion. Color data were also calculated according the National Bureau of Standards (NBS). Results were analyzed statistically by ANOVA and Tukey's HSD test (α=0.05). AP (2.34 ± 0.41) caused color alteration significantly higher than C2 (0.39 ± 0.30) and SH (1.73 ± 0.52). The mean ΔE values were classified as indicial for C2 (0.36 ± 0.29) and noticeable for AP (2.12 ± 0.39) and SH (1.59 ± 0.48). SH (0.0195 ± 0.0150) caused significantly higher ΔRa (p=0.000) than the C2 (0.0005 ± 0.0115) and PA (0.0005 ± 0.0157) groups. There was no statistically significant difference (p=0.063) among the solutions for flexural strength (C1: 105.43 ± 14.93, C2: 100.30 ± 12.43, PA: 97.61 ± 11.09, SH: 95.23 ± 10.18). In conclusion, overnight immersion in denture cleansing solutions simulating a year and a half of use did not alter the flexural strength of acrylic resin but caused noticeable color alterations, higher for alkaline peroxide. The 0.5% NaOCl solution caused increase in surface roughness.
本研究评估了丙烯酸树脂试件在模拟浸泡使用一年半时间的碱性过氧化物和碱性次氯酸盐中浸泡后的颜色稳定性、表面粗糙度和弯曲强度。用热聚合丙烯酸树脂(Lucitone 550)制备了60个圆盘形试件(16×4mm)和80个矩形试件(65×10×3.3mm),并将其分为4组(n = 20):C1组:不浸泡;C2组:在蒸馏水中浸泡8小时;AP组:在碱性过氧化物泡腾片中浸泡8小时;SH组:在0.5%次氯酸钠溶液中浸泡8小时。在基线期和浸泡后对各项性能进行评估。还根据国家标准局(NBS)计算颜色数据。结果采用方差分析和Tukey's HSD检验进行统计学分析(α = 0.05)。AP组(2.34±0.41)导致的颜色变化显著高于C2组(0.39±0.30)和SH组(1.73±0.52)。C2组的平均ΔE值被归类为不明显(0.36±0.29),AP组(2.12±0.39)和SH组(1.59±0.48)为明显。SH组(0.0195±0.0150)导致的ΔRa显著高于C2组(0.0005±0.0115)和PA组(0.0005±0.0157)(p = 0.000)。各溶液组之间的弯曲强度无统计学显著差异(p = 0.063)(C1组:105.43±14.93,C2组:100.30±12.43,PA组:97.61±11.09,SH组:95.23±10.18)。总之,模拟使用一年半的假牙清洁溶液过夜浸泡不会改变丙烯酸树脂的弯曲强度,但会导致明显的颜色变化,碱性过氧化物导致的变化更大。0.5%次氯酸钠溶液会导致表面粗糙度增加。