Hardan L S, Amm E W, Ghayad A, Ghosn C, Khraisat A
Dpt of Restorative Dentistry, School of Dental Medicine, Saint-Joseph University, Beirut, Lebanon.
Odontostomatol Trop. 2009 Jun;32(126):29-37.
To reduce the polymerization shrinkage of the composite resins and after the introduction of the "slow and gradual polymerization" by GORACCI et al. in 1992, many light curing units (LCU) presented the "soft-start polymerization" in addition to the classical high light intensity mode. This study investigated whether this slow and gradual polymerization has the ability of reducing the marginal debonding, by minimizing the internal stress of the composite, knowing that rare are the studies which compared this mode of polymerization.
One hundred twenty Class II cavities were prepared at the mesial and the distal side of human extracted premolars. The teeth were randomly divided into four groups (n = 15). In each tooth the mesial Class II cavities were restored with the micro-hybrid resin composite Filtek Z250 (3M ESPE) and the distal Class II cavities were restored with the nano-filled resin composite Filtek Supreme (3M ESPE). The light curing unit used in this study was a conventional quartz tungsten halogen (QTH) curing light, the QHL 75 (Dentsply) modified by adding a regulating electronic device, controlled by a special software that gives 4 different modes of polymerization as follows: Group A: Standard polymerization: Exposure for 20 seconds at 700 mW/cm2, this group was used as control. Group B: Modified pulse-delay polymerization: Exposure for 2 seconds at 700 mW/cm2, 5 seconds at 0 mW/cm2, then 20 seconds at 700mW/cm2. Group C: Modified ramp polymerization: Exposure for 20 seconds with a slow rise of the intensity to reach the 700 mW/cm2 then 20 seconds at 700 mW/cm2. Group D: Slow and Gradual polymerization: Exposure for 4 minutes with a slow rise of the intensity to reach 700 mW/cm2. The teeth were stored in water at 37 degrees C for 48 hours, then finished and subjected to thermocycling (3000 cycles between 5 degrees C and 55 degrees C). All the teeth were immersed in 2% methylene blue solution for 12 hours at 37 degrees C, sectioned, and evaluated at the gingival margins. Data were statistically analyzed by two-way analysis of variance followed by Tukey HSD multiple comparisons.
The main effect for the type of composites (p = 0.682), and the interaction effect (p = 0.678) did not reach statistical significance. There was a statistically significant main effect for the type of polymerization used (p = 0.014). Post-hoc comparisons using the Tukey HSD test indicated that the mean score for the Group A (M = 2.40, SD = 1.102) was significantly different from the group D (M = 1.30, SD = 1.393, p = 0.010). The group D did not differ significantly from group B (M = 1.63, SD = 1.351, p = 0.767), and group C (M = 1.60, SD = 1.404, p = 0.819). There was a difference between the group A (M = 2.40, SD = 1.102), group B (M = 1.63, SD = 1.351) and group C (M = 1.60, SD = 1.404). However, when the Tukey HSD was used, no statistically significant differences between Group A, B and C were found (p = 0.122 and p = 0.098).
There was a statistically significant difference in microleakage between the "slow and gradual polymerization" and the standard polymerization, however no significant differences were found when using the nano-filled or the micro-hybrid composite materials cured with different polymerization regimens.
为降低复合树脂的聚合收缩率,自1992年戈拉奇等人提出“缓慢渐进聚合”后,许多光固化设备(LCU)除了经典的高光强模式外,还具备“软启动聚合”功能。鉴于比较这种聚合模式的研究较少,本研究旨在探究这种缓慢渐进聚合是否具有通过最小化复合材料内部应力来降低边缘脱粘的能力。
在人类拔除的前磨牙的近中侧和远中侧制备120个II类洞。将牙齿随机分为四组(n = 15)。在每颗牙齿中,近中II类洞用微混合树脂复合材料Filtek Z250(3M ESPE)修复,远中II类洞用纳米填充树脂复合材料Filtek Supreme(3M ESPE)修复。本研究中使用的光固化设备是一台传统的石英钨卤素(QTH)固化灯,即通过添加调节电子装置进行改装的QHL 75(登士柏),由特殊软件控制,该软件提供4种不同的聚合模式,具体如下:A组:标准聚合:在700 mW/cm²下照射20秒,该组用作对照。B组:改良脉冲延迟聚合:在700 mW/cm²下照射2秒,在0 mW/cm²下照射5秒,然后在700 mW/cm²下照射20秒。C组:改良斜坡聚合:强度缓慢上升至700 mW/cm²并照射20秒,然后在700 mW/cm²下照射20秒。D组:缓慢渐进聚合:强度缓慢上升至700 mW/cm²并照射4分钟。将牙齿在37℃水中储存48小时,然后进行修整并进行热循环(在5℃和55℃之间循环3000次)。所有牙齿在37℃下浸入2%亚甲蓝溶液中12小时,切片,并在牙龈边缘进行评估。数据采用双向方差分析,随后进行Tukey HSD多重比较进行统计学分析。
复合材料类型的主效应(p = 0.682)和交互效应(p = 0.678)未达到统计学显著性。所使用的聚合类型存在统计学显著的主效应(p = 0.014)。使用Tukey HSD检验进行事后比较表明,A组(M = 2.40,SD = 1.102)的平均得分与D组(M = 1.30,SD = 1.393,p = 0.010)有显著差异。D组与B组(M = 1.63,SD = 1.351,p = 0.767)和C组(M = 1.60,SD = 1.404,p = 0.819)无显著差异。A组(M = 2.40,SD = 1.102)、B组(M = 1.63,SD = 1.351)和C组之间存在差异。然而,当使用Tukey HSD检验时,未发现A组、B组和C组之间存在统计学显著差异(p = 0.122和p = 0.098)。
“缓慢渐进聚合”与标准聚合之间在微渗漏方面存在统计学显著差异,然而,当使用不同聚合方案固化的纳米填充或微混合复合材料时,未发现显著差异。