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原子探针层析术的空间分辨率。

Spatial resolution in atom probe tomography.

机构信息

Australian Key Centre for Microscopy & Microanalysis, The University of Sydney, NSW 2006, Australia.

出版信息

Microsc Microanal. 2010 Feb;16(1):99-110. doi: 10.1017/S1431927609991267.

Abstract

This article addresses gaps in definitions and a lack of standard measurement techniques to assess the spatial resolution in atom probe tomography. This resolution is known to be anisotropic, being better in-depth than laterally. Generally the presence of atomic planes in the tomographic reconstruction is considered as being a sufficient proof of the quality of the spatial resolution of the instrument. Based on advanced spatial distribution maps, an analysis methodology that interrogates the local neighborhood of the atoms within the tomographic reconstruction, it is shown how both the in-depth and the lateral resolution can be quantified. The influences of the crystallography and the temperature are investigated, and models are proposed to explain the observed results. We demonstrate that the absolute value of resolution is specimen specific.

摘要

本文讨论了原子探针层析技术中分辨率定义上的差距和缺乏标准测量技术的问题。众所周知,这种分辨率具有各向异性,在深度方向上优于横向。一般来说,在层析重建中存在原子面被认为是仪器空间分辨率质量的充分证明。基于先进的空间分布图谱,本文提出了一种分析方法,通过分析层析重建中原子的局部邻域,可以定量确定深度和横向分辨率。研究了晶体学和温度的影响,并提出了模型来解释观察到的结果。我们证明了分辨率的绝对值是特定于样本的。

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