Stender P, Oberdorfer C, Artmeier M, Pelka P, Spaleck F, Schmitz G
Institute of Material Physics, Westf. Willhelms-Universität Münster, Willhelm-Klemm-Str. 10, D-48149 Münster, Germany.
Ultramicroscopy. 2007 Sep;107(9):726-33. doi: 10.1016/j.ultramic.2007.02.032. Epub 2007 Mar 6.
Currently atom probe tomography provides the highest spatial resolution compared to all other volume analysis techniques. Owing to its single atom sensitivity, it is specially suited to study nano-structured materials. Therefore, a new atom probe was installed at the Institute for Material Physics at University of Muenster, Germany, to study thin film reactions. Since the available budget was rather limited, a cost-effective non-commercial atom probe was constructed. The instrument is based on a 2D delay line detector system of 120 mm diameter. To achieve a large collecting angle and thus large volumes of analysis, a straight flight tube without a reflectron is used. This way, the flight distance may be reduced down to 160 mm. However, the variable chamber layout allows using a reflectron as an alternative. Furthermore, a laser system is implemented that delivers pulses in the 500 ps range to make possible laser-assisted evaporation of atoms. The article describes instrumental details and presents first characteristic data.
目前,与所有其他体积分析技术相比,原子探针层析成像具有最高的空间分辨率。由于其单原子灵敏度,它特别适合于研究纳米结构材料。因此,德国明斯特大学材料物理研究所安装了一台新的原子探针,用于研究薄膜反应。由于可用预算相当有限,构建了一种经济高效的非商业原子探针。该仪器基于一个直径为120毫米的二维延迟线探测器系统。为了实现大收集角从而进行大量分析,使用了没有反射镜的直管飞行管。通过这种方式,飞行距离可缩短至160毫米。然而,可变的腔室布局允许使用反射镜作为替代方案。此外,还实施了一个激光系统,该系统能产生500皮秒范围内的脉冲,以使原子的激光辅助蒸发成为可能。本文描述了仪器细节并给出了首批特征数据。