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以甲基丙烯酰氧锆氧簇合物为前驱体制备低温合成多孔锆（IV）二羧酸酯。

A zirconium methacrylate oxocluster as precursor for the low-temperature synthesis of porous zirconium(IV) dicarboxylates.

机构信息

Institut Lavoisier, UMR CNRS 8180, Université de Versailles Saint-Quentin, 78035 Versailles cedex, France.

出版信息

Chem Commun (Camb). 2010 Feb 7;46(5):767-9. doi: 10.1039/b914919h. Epub 2009 Dec 10.

DOI:10.1039/b914919h
PMID:20087514
Abstract

The exchange of the monocarboxylate ligand of the zirconium methacrylate oxocluster Zr(6)O(4)(OH)(4)(OMc)(12) (OMc = CH(2)=CH(CH(3))COO) with dicarboxylic acids (trans,trans muconic acid and terephthalic acid) leads to porous zirconium dicarboxylates exhibiting the UiO-66 architecture; the mild reaction conditions allow the control of their particle size.

摘要

锆甲基丙烯酸盐氧簇 Zr(6)O(4)(OH)(4)(OMc)(12)（OMc = CH(2)=CH(CH(3))COO）的单羧酸配体与二羧酸（反式,反式乌头酸和对苯二甲酸）交换得到具有 UiO-66 结构的多孔锆二羧酸；温和的反应条件允许控制其粒径。

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