Institute of Pharmaceutical Industry of Shandong Province, Jinan, PR China.
Spectrochim Acta A Mol Biomol Spectrosc. 2010 Mar;75(3):1159-62. doi: 10.1016/j.saa.2009.12.082. Epub 2010 Jan 6.
The structure of (1alpha, 2beta, 4beta, 5alpha, 7beta)-7-[(hydroxydi-2-thienylacetyl) oxy]-9,9-dimethyl-3-oxa-9-azoniatricyclo [3.3.1.0(2,4)] nonane bromide monohydrate was studied using 1D and 2D NMR techniques. Complete NMR assignments of the compound were obtained using DEPT, H-H COSY, as well as HMQC and HMBC heteronuclear correlation techniques.
使用 1D 和 2D NMR 技术研究了(1alpha,2beta,4beta,5alpha,7beta)-7-[(羟基二-2-噻吩乙酰基)氧基]-9,9-二甲基-3-氧代-9-氮杂三环[3.3.1.0(2,4)]壬烷溴化物一水合物的结构。使用 DEPT、H-H COSY 以及 HMQC 和 HMBC 异核相关技术,获得了该化合物的完整 NMR 分配。