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基质固相分散萃取的最新进展。

Recent developments in matrix solid-phase dispersion extraction.

机构信息

Dipartimento di Chimica, Sapienza Università di Roma, Box n degrees 34 - Roma 62, Piazzale Aldo Moro 5, 00185 Rome, Italy.

出版信息

J Chromatogr A. 2010 Apr 16;1217(16):2521-32. doi: 10.1016/j.chroma.2010.01.030. Epub 2010 Jan 18.

Abstract

Matrix solid-phase dispersion is a sample preparation strategy widely applied to solid, semisolid or viscous samples, including animal tissues and foods with a high lipidic content. The process consists in blending the matrix onto a solid support, allowing the matrix cell disruption and the subsequent extraction of target analytes by means of a suitable elution solvent. First introduced in 1989, MSPD employment and developments are still growing because of the feasibility and versatility of the process, as evidenced by the several reviews that have been published since nineties. Therefore, the aim of the present review is to provide a general overview and an update of the last developments of MSPD.

摘要

基质固相分散是一种广泛应用于固体、半固体或粘性样品的样品制备策略,包括含有高脂肪含量的动物组织和食品。该过程包括将基质混合到固体支撑物上,允许基质细胞破裂,然后通过适当的洗脱溶剂提取目标分析物。MSPD 于 1989 年首次引入,由于该过程的可行性和多功能性,其应用和发展仍在不断增长,这一点可以从 90 年代以来发表的多篇综述中得到证明。因此,本综述的目的是提供 MSPD 的最新发展的概述和更新。

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