Department of Endodontics, Baylor College of Dentistry, The Texas A&M University System Health Science Center, Dallas, TX, USA.
J Endod. 2010 Mar;36(3):524-8. doi: 10.1016/j.joen.2009.11.012. Epub 2010 Jan 25.
Mineral trioxide aggregate (MTA), white and gray, has many uses in endodontic therapy but is limited by its difficult handling characteristics. This study compared the physical and chemical properties of white MTA (WMTA) with three experimental root-end filling materials: Capasio (Primus Consulting, Bradenton, FL), Ceramicrete-D (Tulsa Dental Specialties/Argonne National Laboratory, Argonne, IL), and Generex-A (Dentsply Tulsa Dental Specialties, Tulsa, OK).
The setting time and radiopacity were tested using International Organization for Standardization (ISO) 6876 methods. Compressive strength was measured following the ISO 9917 method. The pH of the materials was measured after mixing. A novel test was developed for washout resistance of the materials immediately after placement. Data were compared by analysis of variance and Sidak post hoc analysis (p<0.05) for compressive strength and washout resistance.
The setting time of Generex-A was half that of WMTA. All materials met the ISO 6876 requirements for radiopacity. The compressive strengths after 7 days decreased in this order: Generex-A>Capasio>WMTA>Ceramicrete-D. The initial pH of Capasio and Generex-A were alkaline, similar to WMTA, whereas that of Ceramicrete-D was acidic. Significantly, alternative materials remained in situ after the washout test, whereas WMTA was displaced from the retropreparations.
The clinical handling and washout resistance of the alternative materials were far superior to WMTA. The radiopacity, compressive strength, and washout resistance make Generex-A and Capasio materials suitable for further study. Ceramicrete-D was weaker, less radiopaque, and initially acidic.
矿物三氧化物聚合体(MTA)有白色和灰色两种,在根管治疗中有多种用途,但由于其处理特性困难而受到限制。本研究比较了白色 MTA(WMTA)与三种实验性根管封闭材料的物理和化学性质:Capasio(Primus Consulting,Bradenton,FL)、Ceramicrete-D(Tulsa Dental Specialties/Argonne National Laboratory,Argonne,IL)和 Generex-A(Dentsply Tulsa Dental Specialties,Tulsa,OK)。
采用国际标准化组织(ISO)6876 方法测试凝固时间和射线不透性,采用 ISO 9917 方法测量抗压强度。混合后测量材料的 pH 值。开发了一种新的测试方法,用于测试材料放置后立即的冲洗阻力。采用方差分析和 Sidak 事后分析(p<0.05)比较数据抗压强度和冲洗阻力。
Generex-A 的凝固时间是 WMTA 的一半。所有材料均符合 ISO 6876 对射线不透性的要求。7 天后的抗压强度依次降低:Generex-A>Capasio>WMTA>Ceramicrete-D。Capasio 和 Generex-A 的初始 pH 值呈碱性,与 WMTA 相似,而 Ceramicrete-D 的初始 pH 值呈酸性。值得注意的是,替代材料在冲洗试验后仍留在原处,而 WMTA 则从根管预备体中移位。
替代材料的临床处理和冲洗阻力明显优于 WMTA。射线不透性、抗压强度和冲洗阻力使 Generex-A 和 Capasio 材料适合进一步研究。Ceramicrete-D 强度较弱,射线不透性较差,且初始呈酸性。