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Ag 纳米粉末的火花等离子烧结特性研究。

Characterization of spark plasma sintered Ag nanopowders.

机构信息

Department of Mechanical Engineering, School of Engineering and Physical Sciences, Heriot Watt University, Edinburgh, UK.

出版信息

Nanotechnology. 2010 Mar 19;21(11):115707. doi: 10.1088/0957-4484/21/11/115707. Epub 2010 Feb 22.

Abstract

The low temperature sintering behaviour of nanocrystalline Ag powder (with an average size of 70 nm) was characterized. Using spark plasma sintering (SPS), the Ag nanopowders can be successfully sintered at low pressure for only 5 min without external heating, and the sintering density increases and porosity decreases significantly with increase in the sintering temperature. Nanoindentation has been used to characterize the SPS sintered Ag samples. The mechanisms of the low sintering temperature behaviour of the nano-Ag powder and the nanoscale mechanical performance have been discussed. Compression tests were also used to characterize the mechanical properties of the sintered Ag sample with a maximum strain up to 15%.

摘要

纳米晶 Ag 粉末(平均粒径为 70nm)的低温烧结行为得到了研究。采用火花等离子烧结(SPS),Ag 纳米粉末可以在低压下仅 5min 无需外部加热即可成功烧结,并且随着烧结温度的升高,烧结密度显著增加,孔隙率显著降低。纳米压痕技术用于表征 SPS 烧结的 Ag 样品。讨论了纳米 Ag 粉末低温烧结行为的机制和纳米力学性能。压缩试验也用于表征最大应变为 15%的烧结 Ag 样品的力学性能。

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