Department of General Chemistry, University of Pavia, Pavia, Italy.
J Sep Sci. 2010 Apr;33(8):1115-31. doi: 10.1002/jssc.200900753.
The aim of this review is to provide a general overview on the analytical methods proposed in the last decade for trace fluoroquinolone (FQ) determination in environmental waters. A large number of studies have been developed on this topic in reason of the importance of their monitoring in the studies of environmental mobility and potential degradation pathways. Every step of the analysis has been carefully considered, with a particular attention to sample preparation, in relationship with the problems involved in the analysis of real matrices. The different strategies to minimise interference from organic matter and to achieve optimal sensitivity, especially important in those samples with lower FQ concentrations, were also highlighted. Results and progress in this field have been described and critically commented. Moreover, a worldwide overview on the presence of FQs in the environmental waters has been reported.
本次综述的目的在于提供最近十年中痕量氟喹诺酮(FQ)在环境水样中分析方法的概述。由于在环境流动性和潜在降解途径研究中监测其的重要性,这一主题的大量研究已经开展。分析的每一步都经过了仔细考虑,特别关注与实际基质分析相关的问题的样品制备。还强调了不同的策略,以尽量减少有机物的干扰并实现最佳灵敏度,这在那些 FQ 浓度较低的样品中尤为重要。描述并批判性地评论了该领域的结果和进展。此外,还报告了环境水中 FQs 存在的全球概况。