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光固化方案对双固化核桩树脂复合材料聚合收缩和收缩力的影响。

Influence of light-curing protocols on polymerization shrinkage and shrinkage force of a dual-cured core build-up resin composite.

作者信息

Tauböck Tobias T, Bortolotto Tissiana, Buchalla Wolfgang, Attin Thomas, Krejci Ivo

机构信息

Department of Preventive Dentistry, Periodontology and Cariology, University of Zurich, Zurich, Switzerland.

出版信息

Eur J Oral Sci. 2010 Aug;118(4):423-9. doi: 10.1111/j.1600-0722.2010.00746.x.

Abstract

This study investigated the influence of time delay and duration of photo-activation on linear polymerization shrinkage, shrinkage force, and hardening of a dual-cured core build-up resin composite. The test material (Rebilda DC) was light-cured for 20 or 60 s either early (2 min) or late (7 min) after the start of mixing. Non-irradiated self-cured specimens served as controls. Linear shrinkage and shrinkage force were measured for 60 min using custom-made devices. Knoop hardness was determined at the end of the observation period. Self-cured controls, showing a linear shrinkage similar to that of specimens early light-cured for 20 s generated the lowest shrinkage force and hardness. A shorter light exposure time (20 s vs. 60 s) reduced linear shrinkage, shrinkage force, and hardness when early light-curing was performed, but did not affect the three properties in specimens light-cured late after the start of mixing. Late photo-activation increased linear shrinkage, irrespective of irradiation time, and resulted in a higher shrinkage force and hardness for short light exposure time. A moderate correlation was found between the two shrinkage properties studied (r(2) = 0.65). In conclusion, improvements in shrinkage behavior of the tested core build-up material were associated with inferior hardening, making it important to adapt curing protocols to the clinical situation.

摘要

本研究调查了光活化的时间延迟和持续时间对双固化核成型树脂复合材料的线性聚合收缩、收缩力及固化的影响。测试材料(Rebilda DC)在混合开始后早期(2分钟)或晚期(7分钟)分别进行20秒或60秒的光固化。未辐照的自固化试样用作对照。使用定制装置测量60分钟内的线性收缩和收缩力。在观察期结束时测定努氏硬度。自固化对照试样产生的收缩力和硬度最低,其线性收缩与早期光固化20秒的试样相似。当进行早期光固化时,较短的光照时间(20秒对60秒)可降低线性收缩、收缩力和硬度,但对混合开始后晚期光固化的试样的这三种性能没有影响。无论辐照时间如何,晚期光活化都会增加线性收缩,并且对于短光照时间会导致更高的收缩力和硬度。在所研究的两种收缩性能之间发现了中等程度的相关性(r(2) = 0.65)。总之,测试的核成型材料收缩行为的改善与固化不足相关,这使得根据临床情况调整固化方案很重要。

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