Institute of Scientific Instruments of ASCR, Královopolská, Czech Republic.
J Microsc. 2010 Sep 1;239(3):233-8. doi: 10.1111/j.1365-2818.2010.03377.x.
We present results obtained with a new scintillation detector of secondary electrons for the variable pressure scanning electron microscope. A detector design is based on the positioning of a single crystal scintillator within a scintillator chamber separated from the specimen chamber by two apertures. This solution enables us to decrease the pressure to several Pa in the scintillator chamber while the pressure in the specimen chamber reaches values of about 1000 Pa (7.5 Torr). Due to decreased pressure, we can apply a potential of the order of several kV to the scintillator, which is necessary for the detection of secondary electrons. Simultaneously, the two apertures at appropriate potentials of the order of several hundreds of volts create an electrostatic lens that allows electrons to pass from the specimen chamber to the scintillator chamber. Results indicate a promising utilization of this detector for a wide range of specimen observations.
我们展示了一种新型闪烁体二次电子扫描电子显微镜变压探测器的结果。探测器的设计基于在闪烁体室内定位单个晶体闪烁体,该闪烁体室通过两个孔径与试样室隔开。这种解决方案使我们能够将闪烁体室内的压力降低到几个帕斯卡,而试样室内的压力达到约 1000 帕斯卡(7.5 托)。由于压力降低,我们可以在闪烁体上施加几千伏的电势,这对于检测二次电子是必要的。同时,两个孔径在几百伏特的适当电势下形成静电透镜,允许电子从试样室穿过到闪烁体室。结果表明,这种探测器在广泛的试样观察中具有广阔的应用前景。