Dental Biomaterials Department, Faculty of Dentistry, Mansoura University, Al Gomhoria Street, Mansoura, Egypt.
J Mech Behav Biomed Mater. 2010 Nov;3(8):610-8. doi: 10.1016/j.jmbbm.2010.07.011. Epub 2010 Jul 27.
The aim of this study was to evaluate fracture toughness, hardness, ceramic/metal bond strength and microstructure of experimental dental porcelain and compare it with commercial type. Specimens of specific dimensions were prepared. Fracture toughness was assessed by a three-point bending test. The Vickers hardness was measured using a microhardness tester. The ceramometal bond strength was measured using a universal testing machine. The load was applied at the porcelain/metal interface via a chisel edged blade with a crosshead speed of 2.0 mm/min until fracture. The polished specimens of dental porcelain were chemically etched and the microstructure was analyzed with a scanning electron microscope. The results showed comparable fracture toughness and bond strength for both materials, while the experimental porcelain exhibited higher hardness. The experimental porcelain showed uniform cohesive failure while the commercial type showed mixed mode of failure. The microstructure of the experimental porcelain was tetragonal leucite crystals dispersed randomly in a glass matrix. The leucite crystals exist in two forms, acicular and rod like structures. It was concluded that the experimental porcelain has adequate fracture toughness and ceramic/metal bond strength that can resist the rapid crack propagation and its consequent catastrophic failure, which indicates a material serviceability in the oral cavity.
本研究旨在评估实验性牙科瓷的断裂韧性、硬度、陶瓷/金属结合强度和微观结构,并将其与商业性瓷进行比较。制备了特定尺寸的标本。通过三点弯曲试验评估断裂韧性。使用显微硬度计测量维氏硬度。使用万能试验机测量陶瓷/金属结合强度。通过带有刃口的凿子以 2.0mm/min 的十字头速度在瓷/金属界面施加负载,直至断裂。对牙科瓷的抛光标本进行化学蚀刻,并用扫描电子显微镜分析微观结构。结果表明,两种材料的断裂韧性和结合强度相当,而实验性瓷的硬度较高。实验性瓷表现出均匀的内聚性破坏,而商业性瓷则表现出混合破坏模式。实验性瓷的微观结构为随机分散在玻璃基质中的四方型白榴石晶体。白榴石晶体以针状和棒状结构存在两种形式。结论是,实验性瓷具有足够的断裂韧性和陶瓷/金属结合强度,可以抵抗快速裂纹扩展及其随后的灾难性失效,这表明该材料在口腔中有良好的适用性。