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通过射频磁控溅射沉积的极紫外Mo/Si多层膜反射镜。

Extreme-ultraviolet Mo/Si multilayer mirrors deposited by radio-frequency-magnetron sputtering.

作者信息

Montcalm C, Sullivan B T, Pépin H, Dobrowolski J A, Sutton M

出版信息

Appl Opt. 1994 Apr 1;33(10):2057-68. doi: 10.1364/AO.33.002057.

Abstract

Mo/Si multilayer mirrors with a high reflectance at normal incidence in the 130-135-Å spectral region have been deposited by rf magnetron sputtering. A new and quick technique was used to calibrate the deposition rates. Characterization by transmission electron microscopy (TEM) and grazing-incidence x-ray diffraction (XRD) indicated good thickness control of the deposition process and low interface roughness. However, the TEM and, indirectly, the XRD reflectance measurements, indicated that the interfaces are asymmetric. A brief review discussing the origin of the modulation of the Bragg peak intensities in the XRD reflectance is given. An analytical formula was derived for periodic multilayers that describes the effect of asymmetric interfaces on the amplitude of the Bragg peak modulation. Theoretically, in XRD reflectance measurements, any asymmetry in the interdiffusion of the Mo-Si interfaces results in a decrease of the usual amplitude modulation of the Bragg peaks. Extreme-ultraviolet (XUV) reflectance measurements were also made with synchrotron radiation on a new high-resolution reflectometer. The near-normal-incidence peak reflectances measured at λ = 134 Å were ~ 59% for the best multilayer mirrors. Good fits to both XRD and XUV reflectance measurements have been obtained with a model that allows for interface asymmetry.

摘要

通过射频磁控溅射沉积了在130 - 135埃光谱区域正入射时具有高反射率的Mo/Si多层镜。采用了一种新的快速技术来校准沉积速率。通过透射电子显微镜(TEM)和掠入射X射线衍射(XRD)进行表征,结果表明沉积过程的厚度控制良好且界面粗糙度较低。然而,TEM以及间接的XRD反射率测量表明界面是不对称的。给出了一篇简短综述,讨论了XRD反射率中布拉格峰强度调制的起源。推导了一个用于周期性多层膜的解析公式,该公式描述了不对称界面对布拉格峰调制幅度的影响。从理论上讲,在XRD反射率测量中,Mo - Si界面互扩散中的任何不对称都会导致布拉格峰通常的幅度调制减小。还利用同步辐射在一台新型高分辨率反射计上进行了极紫外(XUV)反射率测量。对于最佳的多层镜,在λ = 134埃处测量的近正入射峰值反射率约为59%。利用一个考虑界面不对称性的模型,已获得与XRD和XUV反射率测量结果的良好拟合。

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