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芒果叶辅助合成分散良好的银纳米粒子。

Mangifera indica leaf-assisted biosynthesis of well-dispersed silver nanoparticles.

机构信息

Department of Physics, Mar Ivanios College, Thiruvananthapuram 695015, India.

出版信息

Spectrochim Acta A Mol Biomol Spectrosc. 2011 Jan;78(1):327-31. doi: 10.1016/j.saa.2010.10.015. Epub 2010 Oct 27.

Abstract

The use of various parts of plants for the synthesis of nanoparticles is considered as a green technology as it does not involve any harmful chemicals. The present study reports a facile and rapid biosynthesis of well-dispersed silver nanoparticles. The method developed is environmentally friendly and allows the reduction to be accelerated by changing the temperature and pH of the reaction mixture consisting of aqueous AgNO3 and Mangifera Indica leaf extract. At a pH of 8, the colloid consists of well-dispersed triangular, hexagonal and nearly spherical nanoparticles having size ∼20 nm. The UV-vis spectrum of silver nanoparticles gave surface plasmon resonance (SPR) at 439 nm. The synthesized nanocrystals were characterized using transmission electron microscopy (TEM), X-ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy. Water soluble organics present in the leaf are responsible for the reduction of silver ions. This green method provides faster synthesis comparable to chemical methods and can be used in areas such as cosmetics, foods and medical applications.

摘要

将植物的各个部分用于合成纳米粒子被认为是一种绿色技术,因为它不涉及任何有害化学物质。本研究报告了一种简便、快速的银纳米粒子的生物合成方法。所开发的方法环保,并且可以通过改变包含水性 AgNO3 和芒果叶提取物的反应混合物的温度和 pH 值来加速还原。在 pH 值为 8 的情况下,胶体由尺寸约为 20nm 的良好分散的三角形、六边形和近球形纳米粒子组成。银纳米粒子的紫外-可见光谱在 439nm 处给出了表面等离子体共振(SPR)。使用透射电子显微镜(TEM)、X 射线衍射(XRD)和傅里叶变换红外(FTIR)光谱对合成的纳米晶体进行了表征。叶片中存在的水溶性有机物负责还原银离子。这种绿色方法提供了与化学方法相当的更快的合成速度,可以用于化妆品、食品和医疗应用等领域。

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