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声空化化学:使用可重复使用的硅胶氯化物作为催化剂,在超声条件下温和高效地合成酰胺基烷基-2-萘酚的多组分方法。

Cavitational chemistry: a mild and efficient multi-component synthesis of amidoalkyl-2-naphthols using reusable silica chloride as catalyst under sonic conditions.

机构信息

Department of Studies in Chemistry, Central College Campus, Bangalore University, Bengaluru, India.

出版信息

Ultrason Sonochem. 2011 Mar;18(2):624-8. doi: 10.1016/j.ultsonch.2010.09.011. Epub 2010 Oct 8.

Abstract

An efficient and direct procedure for the synthesis of amidoalkyl-2-naphthol derivatives has been described. The process employs a three-component cyclocondensation reaction in one-pot using β-naphthol, aromatic aldehyde and acetamide or benzamide in the presence of silica chloride accelerated by ultrasound giving the product in excellent yield in very short duration.

摘要

描述了一种高效、直接的合成酰胺基-2-萘酚衍生物的方法。该方法采用β-萘酚、芳香醛和乙酰胺或苯甲酰胺在硅胶氯化物存在下超声促进的一锅法三组分环缩合反应,以极好的收率在极短的时间内得到产物。

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