Yang Hong-Shen, Hua Yong-Li, Guo Yan-Sheng, Du Tian-Xi, Yang Xiao-Hu, Qinh Liang, Qu Ya-Ling, Wei Yan-Ming
College of Veterinary Medicine,Gansu Agriculture University, Lanzhou 730070, China.
Zhong Yao Cai. 2010 Jun;33(6):874-8.
To establish the quality standard of oil-processed Radix Angelica sinensis.
Combined traditional identification, TLC and fingerprints of wine-processed Radix Angelica sinensis to control quality of oil-processed Radix Angelica sinensis. And referring to China Pharmacopoeia of 2005 edition, water, ash, and extract were also detected.
The content of water, total ash, extract representatively was 7.30%, 8.70% and 50.9%. Eleven fingerprint peaks were defined, The eleven common peaks were appointed as fingerprint peaks by analyzing 14 representative samples, all the fingerprint peaks were quantified grounded on the peak of Ferulic acid. and quantified rested on the peak of ferulic acid.
A multicomponent quantitative method for oil-processed Radix Angelica sinensis is established. The established method is feasible. The quality control standards of the oil-processed Radix Angelica sinensis is normative, systematic and accurate.
建立当归炮制后的质量标准。
结合传统鉴别、薄层色谱法(TLC)和当归酒炙品指纹图谱来控制当归炮制后的质量。并参照《中国药典》2005年版,对水分、灰分和浸出物进行检测。
水分、总灰分、浸出物的代表性含量分别为7.30%、8.70%和50.9%。确定了11个指纹峰,通过分析14个代表性样品,将这11个共有峰指定为指纹峰,所有指纹峰均以阿魏酸峰为基准进行定量。
建立了当归炮制后的多成分定量方法。所建立的方法可行。当归炮制后的质量控制标准规范、系统且准确。