Ziaie F, Hajiloo N, Alipour A, Amraei R, Mehtieva S I
Agricultural, Medical and Industrial Research School, Nuclear Science and Technology Research Institute, PO Box 31485-498, Karaj, Iran.
Radiat Prot Dosimetry. 2011 Jun;145(4):377-84. doi: 10.1093/rpd/ncq443. Epub 2010 Dec 4.
Micro and nano-structure hydroxyapatite samples were synthesized via several different methods. The samples were characterised utilising the Fourier transmission infra-red, scanning electron microscope and X-ray diffraction methods, to find out the structure most similar to human tooth enamel, and the best method was found. The electron paramagnetic resonance (EPR) signals of the gamma-irradiated samples were measured using an EPR spectrometer system. A calibration curve was established by irradiation of the samples at four doses of 50-500 mGy. The parameters of the calibration curve, slope and intercept with dose axis are determined by linear regression analysis. This calibration curve can be used for human tooth enamel for retrospective dosimetry purposes.
通过几种不同方法合成了微米和纳米结构的羟基磷灰石样品。利用傅里叶透射红外光谱、扫描电子显微镜和X射线衍射方法对样品进行了表征,以找出与人类牙釉质最相似的结构,并找到了最佳方法。使用电子顺磁共振(EPR)光谱仪系统测量了γ辐照样品的电子顺磁共振(EPR)信号。通过对样品进行50-500 mGy的四个剂量照射建立了校准曲线。校准曲线的参数、斜率和与剂量轴的截距通过线性回归分析确定。该校准曲线可用于人类牙釉质的回顾性剂量测定。