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Doxofyllinium tetra-chloridoanti-monate(III) monohydrate.

作者信息

Wei Wan Xing, Feng Wen-Jie, Zheng Bo-Jiöng, Chen Ying, Jin Zhi-Min

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2007 Dec 12;64(Pt 1):m167. doi: 10.1107/S1600536807065774.

DOI:10.1107/S1600536807065774
PMID:21200515
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2915103/
Abstract

The title compound, (C(11)H(14)N(4)O(4))[SbCl(4)]·H(2)O, comprises a protonated doxofyllinium cation [7-(1,3-dioxolan-2-ylmeth-yl)-1,3-dimethyl-2,6-dioxo-3,7-dihydro-1H-purin-9-ium], an SbCl(4) anion and a water mol-ecule linked by N-H⋯O and O-H⋯Cl hydrogen bonds: the SbCl(4) anions form centrosymmetric dimers via weak Sb⋯Cl inter-actions [Sb⋯Cl = 3.1159 (9) Å]. The geometrical arrangement in the crystal structure is characterized by slipped π-π stacking of the parallel purine ring systems, with an inter-planar separation of 3.32 Å.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/5485ae25bbf1/e-64-0m167-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/c65ed494d0b2/e-64-0m167-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/07321a8563b0/e-64-0m167-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/5485ae25bbf1/e-64-0m167-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/c65ed494d0b2/e-64-0m167-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/07321a8563b0/e-64-0m167-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/6397/2915103/5485ae25bbf1/e-64-0m167-fig3.jpg

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