• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

4-羟基苯甲醛的重新测定

Redetermination of 4-hydroxy-benzaldehyde.

作者信息

Jasinski Jerry P, Butcher Ray J, Narayana B, Swamy M T, Yathirajan H S

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2007 Dec 6;64(Pt 1):o187. doi: 10.1107/S1600536807063659.

DOI:10.1107/S1600536807063659
PMID:21200751
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2915250/
Abstract

This is a redetermination of the structure of the title compound, C(7)H(6)O(2), which was first reported by Iwasaki [Acta Cryst. (1977 ▶), B33, 1646-1648]. The results are obtained with greater precision in the present study. Crystal packing is stabilized by inter-molecular O-H⋯O inter-actions between the hydroxyl and aldehyde groups which link the mol-ecules into chains in a zigzag pattern along the [110] plane of the unit cell.

摘要

这是对标题化合物C₇H₆O₂结构的重新测定，该化合物最早由岩崎报道[《晶体学报》(1977年 ▶)，B33，1646 - 1648]。在本研究中获得了更高精度的结果。晶体堆积通过羟基和醛基之间的分子间O—H⋯O相互作用得以稳定，这些相互作用将分子沿晶胞的[110]平面以之字形模式连接成链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5cfb/2915250/7ab4173b4c60/e-64-0o187-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5cfb/2915250/ce43c3041188/e-64-0o187-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5cfb/2915250/7ab4173b4c60/e-64-0o187-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5cfb/2915250/ce43c3041188/e-64-0o187-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5cfb/2915250/7ab4173b4c60/e-64-0o187-fig2.jpg

相似文献

1
Redetermination of 4-hydroxy-benzaldehyde.4-羟基苯甲醛的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2007 Dec 6;64(Pt 1):o187. doi: 10.1107/S1600536807063659.
2
Redetermination of 3-methyl-benzoic acid.3-甲基苯甲酸的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2011 Feb 5;67(Pt 3):o569-70. doi: 10.1107/S1600536811003849.
3
Redetermination of 1-naphthalene-acetic acid.1-萘乙酸的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 13;64(Pt 12):o2310. doi: 10.1107/S1600536808036246.
4
5-Diethyl-amino-2-[(E)-(4-methyl-3-nitro-phenyl)-imino-meth-yl]phenol: a redetermination.5-二乙氨基-2-[(E)-(4-甲基-3-硝基苯基)-亚氨基甲基]苯酚：重新测定
Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 17;65(Pt 2):o349-50. doi: 10.1107/S1600536809001731.
5
Redetermination of loperamide monohydrate.洛哌丁胺一水合物的重新测定。
Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):o539-40. doi: 10.1107/S1600536812003091. Epub 2012 Jan 31.
6
Redetermination of (E)-3-(anthracen-9-yl)-1-(2-hy-droxy-phen-yl)prop-2-en-1-one.（E）-3-（蒽-9-基）-1-（2-羟基苯基）丙-2-烯-1-酮的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2011 Oct 1;67(Pt 10):o2554-5. doi: 10.1107/S1600536811034994. Epub 2011 Sep 3.
7
2,2'-Dithio-dianiline: a redetermination at 100 K.2,2'-二硫代二苯胺：在100K下的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2010 Jan 9;66(Pt 2):o292-3. doi: 10.1107/S1600536810000024.
8
Redetermination of 2-[4-(2-hydroxy-ethyl)piperazin-1-ium-1-yl]ethanesul-fonate at 100 K.在100K下对2-[4-(2-羟乙基)哌嗪-1-鎓-1-基]乙烷磺酸盐进行重新测定。
Acta Crystallogr Sect E Struct Rep Online. 2009 Nov 7;65(Pt 12):o3027-8. doi: 10.1107/S1600536809042512.
9
Redetermination of 3-deaza-uracil.3-脱氮尿嘧啶的重新测定
Acta Crystallogr Sect E Struct Rep Online. 2008 May 17;64(Pt 6):o1107-8. doi: 10.1107/S1600536808014578.
10
A monoclinic polymorph of 1-benzoyl-4-thio-biuret.1-苯甲酰基-4-硫代缩二脲的一种单斜晶多晶型物。
Acta Crystallogr Sect E Struct Rep Online. 2013 Nov 13;69(Pt 12):o1760. doi: 10.1107/S1600536813030250.

引用本文的文献

1
Crystal engineering of a 1:1 5-fluoro-cytosine-4-hy-droxy-benzaldehyde cocrystal: insights from X-ray crystallography and Hirshfeld analysis.1:1 5-氟胞嘧啶-4-羟基苯甲醛共晶体的晶体工程：来自X射线晶体学和 Hirshfeld 分析的见解
Acta Crystallogr E Crystallogr Commun. 2025 May 23;81(Pt 6):549-553. doi: 10.1107/S2056989025004463. eCollection 2025 Jun 1.
2
Quantum Chemical Lipophilicities of Antimalarial Drugs in Relation to Terminal Half-Life.抗疟药物的量子化学亲脂性与终末半衰期的关系
ACS Omega. 2020 Mar 23;5(12):6500-6515. doi: 10.1021/acsomega.9b04140. eCollection 2020 Mar 31.
3
4-Hydr-oxy-3-nitro-benzaldehyde.

本文引用的文献

1
Montmorillonite KSF as an Inorganic, Water Stable, and Reusable Catalyst for the Knoevenagel Synthesis of Coumarin-3-carboxylic Acids.蒙脱石KSF作为一种无机、水稳定且可重复使用的催化剂用于Knoevenagel合成香豆素-3-羧酸
J Org Chem. 1999 Feb 5;64(3):1033-1035. doi: 10.1021/jo981794r.
2
3-Hydroxybenzaldehyde.3-羟基苯甲醛
Acta Crystallogr C. 2000 Nov;56 Pt 11:1348-50. doi: 10.1107/s0108270100010441.
3
C-H.pi interactions in 9-(n-dodecylaminomethyl)anthracene.9 -（正十二烷基氨基甲基）蒽中的C-H…π相互作用
4-羟基-3-硝基苯甲醛
Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 26;64(Pt 5):o915. doi: 10.1107/S1600536808011148.
Acta Crystallogr C. 2000 Sep;56 (Pt 9):1136-8. doi: 10.1107/s0108270100008441.
4
Aldehyde methacrylates derived from hydroxybenzaldehydes.源自羟基苯甲醛的甲基丙烯酸醛酯。
J Dent Res. 1978 Mar;57(3):500-5. doi: 10.1177/00220345780570031801.