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Aqua-tris[6-(3,5-dimethyl-1H-pyrazol-1-yl)picolinato]-κN,N',O;κO-dysprosium(III) trihydrate.

作者信息

Kai Zhao, Yu Feng, Yin Xian-Hong, Jie Zhu, Lin Cui-Wu

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Jan 25;64(Pt 2):m408-9. doi: 10.1107/S1600536808001943.

DOI:10.1107/S1600536808001943
PMID:21201355
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960341/
Abstract

In the title complex, [Dy(C(11)H(10)N(3)O(2))(3)(H(2)O)]·3H(2)O, the Dy(III) atom is coordinated by four N atoms and four O atoms derived from three tridentate deprotonated 6-(3,5-dimethyl-1H-pyrazol-1-yl)picolinate ligands and one water mol-ecule. The complex and solvent water mol-ecules are linked together via O-H⋯O, O-H⋯N, C-H⋯O and C-H⋯π hydrogen-bonding inter-actions, forming a three-dimensional network structure.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a63/2960341/e0c1fa9a5680/e-64-0m408-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a63/2960341/9bdfffbc75d4/e-64-0m408-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a63/2960341/e0c1fa9a5680/e-64-0m408-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a63/2960341/9bdfffbc75d4/e-64-0m408-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8a63/2960341/e0c1fa9a5680/e-64-0m408-fig2.jpg

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本文引用的文献

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A short history of SHELX.SHELX简史。
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