Sikorski Artur, Niziołek Agnieszka, Krzymiński Karol, Lis Tadeusz, Błażejowski Jerzy
Acta Crystallogr Sect E Struct Rep Online. 2008 Jan 4;64(Pt 2):o372-3. doi: 10.1107/S1600536807068109.
The crystal structure of the title compound, C(21)H(15)N(2)O(4) (+)·CF(3)O(3)S(-), is stabilized by C-H⋯O and C-H⋯F hydrogen bonds, by C-F⋯π, N-O⋯π and S-O⋯π inter-actions, and by O⋯O [2.70 (4) Å] and O⋯F [2.85 (1) or 2.92 (1) Å] contacts; π-π interactions are also present. In the packing of the mol-ecules, acridine units are either parallel or inclined at an angle of 12.5 (1)°. The nitrophenoxycarbonyl unit is disordered over two position; the site occupancy factors are 0.89 and 0.11.
标题化合物C(21)H(15)N(2)O(4) (+)·CF(3)O(3)S(-)的晶体结构通过C-H⋯O和C-H⋯F氢键、C-F⋯π、N-O⋯π和S-O⋯π相互作用以及O⋯O [2.70 (4) Å]和O⋯F [2.85 (1) 或2.92 (1) Å]接触得以稳定;同时也存在π-π相互作用。在分子堆积中,吖啶单元要么平行,要么以12.5 (1)°的角度倾斜。硝基苯氧基羰基单元在两个位置上无序;位点占有率因子分别为0.89和0.11。