• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

1-萘基 9H-咔唑-4-磺酸盐

1-Naphthyl 9H-carbazole-4-sulfonate.

作者信息

Arulmozhi R, Vennila Jasmine P, Babu Sunil Manohar, Kavitha Helen P, Manivannan V

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 7;64(Pt 7):o1208. doi: 10.1107/S1600536808016334.

DOI:10.1107/S1600536808016334
PMID:21202847
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961653/
Abstract

In the title compound, C(22)H(15)NO(3)S, the plane of the carbazole ring system forms a dihedral angle of 65.06 (4)° with the naphthalene ring system. In the crystal structure, a weak intra-molecular C-H⋯O inter-action is observed between the naphthalene ring system and the sulfonate group. Two weak inter-molecular C-H⋯O inter-actions are also observed.

摘要

在标题化合物C₂₂H₁₅NO₃S中，咔唑环系平面与萘环系形成的二面角为65.06（4）°。在晶体结构中，观察到萘环系与磺酸酯基团之间存在弱的分子内C-H⋯O相互作用。还观察到两个弱的分子间C-H⋯O相互作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4721/2961653/0f9227ad6717/e-64-o1208-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4721/2961653/49b774b26c69/e-64-o1208-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4721/2961653/0f9227ad6717/e-64-o1208-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4721/2961653/49b774b26c69/e-64-o1208-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4721/2961653/0f9227ad6717/e-64-o1208-fig2.jpg

相似文献

1
1-Naphthyl 9H-carbazole-4-sulfonate.1-萘基 9H-咔唑-4-磺酸盐
Acta Crystallogr Sect E Struct Rep Online. 2008 Jun 7;64(Pt 7):o1208. doi: 10.1107/S1600536808016334.
2
Crystal structures of two new carbazole derivatives: 12-(4-nitro-phen-yl)-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole and 2-methyl-4-(4-nitro-phen-yl)-9-phenyl-sulfonyl-9-thieno[2,3-]carbazole.两种新型咔唑衍生物的晶体结构：12-(4-硝基苯基)-7-苯基磺酰基-7-苯并呋喃并[2,3-]咔唑和2-甲基-4-(4-硝基苯基)-9-苯基磺酰基-9-噻吩并[2,3-]咔唑。
Acta Crystallogr E Crystallogr Commun. 2016 Nov 4;72(Pt 12):1739-1743. doi: 10.1107/S2056989016016996. eCollection 2016 Dec 1.
3
4-Amino-phenyl naphthalene-1-sulfonate.4-氨基-苯基萘-1-磺酸盐
Acta Crystallogr Sect E Struct Rep Online. 2008 May 21;64(Pt 6):o1124. doi: 10.1107/S1600536808014438.
4
4-Nitro-phenyl naphthalene-1-sulfonate.4-硝基-苯基萘-1-磺酸盐
Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 30;64(Pt 9):o1848. doi: 10.1107/S1600536808027396.
5
2,4-Dinitro-1-naphthyl 4-toluene-sulfonate.2,4-二硝基-1-萘基对甲苯磺酸酯
Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 18;64(Pt 5):o873. doi: 10.1107/S1600536808010052.
6
Crystal structures of three carbazole derivatives: 12-ethyl-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole, (1), 2-(4,5-dimeth-oxy-2-nitro-phen-yl)-4-hy-droxy-9-phenyl-sulfonyl-9-carbazole-3-carbaldehyde, (2), and 12-phenyl-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole, (3).三种咔唑衍生物的晶体结构：12-乙基-7-苯基磺酰基-7-苯并呋喃并[2,3-]咔唑，（1）；2-（4,5-二甲氧基-2-硝基苯基）-4-羟基-9-苯基磺酰基-9-咔唑-3-甲醛，（2）；以及12-苯基-7-苯基磺酰基-7-苯并呋喃并[2,3-]咔唑，（3）。
Acta Crystallogr E Crystallogr Commun. 2016 Nov 4;72(Pt 12):1744-1750. doi: 10.1107/S2056989016016819. eCollection 2016 Dec 1.
7
Crystal structure of ethyl 2-phenyl-9-phenyl-sulfonyl-9H-carbazole-3-carboxyl-ate.2-苯基-9-苯基磺酰基-9H-咔唑-3-羧酸乙酯的晶体结构
Acta Crystallogr E Crystallogr Commun. 2015 Sep 12;71(Pt 10):o725-6. doi: 10.1107/S205698901501662X. eCollection 2015 Oct 1.
8
Crystal structure of 2-(2,4-di-chloro-phen-yl)-4-hydroxy-9-phenyl-sulfonyl-9H-carbazole-3-carbaldehyde.2-(2,4-二氯苯基)-4-羟基-9-苯基磺酰基-9H-咔唑-3-甲醛的晶体结构
Acta Crystallogr Sect E Struct Rep Online. 2014 Nov 8;70(Pt 12):466-8. doi: 10.1107/S1600536814024064. eCollection 2014 Dec 1.
9
Methyl 9H-carbazole-9-acetate.9H-咔唑-9-乙酸甲酯
Acta Crystallogr Sect E Struct Rep Online. 2009 Apr 25;65(Pt 5):o1136. doi: 10.1107/S1600536809015141.
10
7,9-Dimethyl-5-phenyl-sulfonyl-5H-benzo[b]carbazole.7,9-二甲基-5-苯基磺酰基-5H-苯并[b]咔唑
Acta Crystallogr Sect E Struct Rep Online. 2008 Aug 6;64(Pt 9):o1667-8. doi: 10.1107/S1600536808024380.

引用本文的文献

1
2,3,4,9-Tetra-hydro-1H-carbazole.2,3,4,9-四氢-1H-咔唑
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 26;64(Pt 12):o2433. doi: 10.1107/S1600536808038713.

本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
Charge-transfer complexes of N-methyl-, N-isopropyl-, N-butyl- and N-isobutylcarbazole with 3,5-dinitrobenzoic acid.N-甲基咔唑、N-异丙基咔唑、N-丁基咔唑和N-异丁基咔唑与3,5-二硝基苯甲酸的电荷转移络合物。
Acta Crystallogr C. 2000 Apr 15;56(Pt 4):E144-6. doi: 10.1107/S010827010000384X.
3
Antioxidative activity of carbazoles from Murraya koenigii leaves.九里香叶中咔唑类化合物的抗氧化活性
J Agric Food Chem. 2001 Nov;49(11):5589-94. doi: 10.1021/jf010621r.
4
Antitumor agents. 203. Carbazole alkaloid murrayaquinone A and related synthetic carbazolequinones as cytotoxic agents.抗肿瘤剂。203. 咔唑生物碱九里香醌A及相关合成咔唑醌作为细胞毒性剂。
J Nat Prod. 2000 Jul;63(7):893-7. doi: 10.1021/np000020e.