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catena-Poly[μ-aqua-2:1'κO:O-aqua-2κO-(2-fluoro-benzoato-1κO,O')(μ(2)-2-fluoro-benzoato-2':1κO:O')bis-(μ(3)-2-fluoro-benzoato)-2':1:2κO:O,O':O';1:2:1'κF,O:O,O':O'-dilead(II)].

作者信息

Zhang Bi-Song

机构信息

College of Materials Science and Chemical Engineering, Jinhua College of Professions and Technology, Jinhua, Zhejiang 321017, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 23;64(Pt 8):m1055-6. doi: 10.1107/S1600536808022678.

DOI:10.1107/S1600536808022678
PMID:21203040
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2961970/
Abstract

In the title compound, Pb(2)(C(7)H(4)FO(2))(4)(H(2)O)(2), one Pb(II) atom is coordinated by seven O atoms and one F atom from five 2-fluoro-benzoate ligands, and the other Pb(II) atom is coordinated by five O atoms from four 2-fluoro-benzoate ligands and three water mol-ecules, resulting in distorted PbO(7)F and PbO(8) polyhedra. The 2-fluoro-benzoate ligands bridge Pb atoms, giving rise to a one-dimensional chain structure extending along the [100] direction. The polymeric chains are connected via C-H⋯O hydrogen bonds and π-π inter-actions, with an inter-planar distance of 3.46 (1) Å. An intramolecular O-H⋯F interaction is also present.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/0ae122b1565a/e-64-m1055-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/eda4b9c2abe8/e-64-m1055-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/14fd807efa8a/e-64-m1055-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/0ae122b1565a/e-64-m1055-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/eda4b9c2abe8/e-64-m1055-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/14fd807efa8a/e-64-m1055-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/4196/2961970/0ae122b1565a/e-64-m1055-fig3.jpg

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引用本文的文献

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本文引用的文献

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A short history of SHELX.SHELX简史。
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