Department of Dental Physical Sciences, Barts and The London School of Medicine and Dentistry, Queen Mary University of London, Mile End, London, E1 4NS, UK.
J Mater Sci Mater Med. 2011 Feb;22(2):247-51. doi: 10.1007/s10856-010-4209-z. Epub 2011 Jan 8.
Ultrasound has been shown to improve the set of glass ionomer cements (GICs) and also other cement properties. In particular, the release of fluoride is enhanced. These cements also can take up fluoride ion from liquids. The aim of this study is to investigate the effect of ultrasound on this cement property. Two commercial dental restorative GICs were used together with a modified commercial material and an experimental material based on a F-free glass. All three commercial materials came in capsules which were mixed as makers directed, the experimental material was mixed as in previous papers. Mixed cement was placed polyethylene moulds to create 3 × 2 mm thick discs. These were either allowed to standard set for 6 min or set with ultrasound for 55 s. 18 samples were made for each material/set. Three samples were placed in 4 ml of 0.2% NaF solution for 24 h at 37°C. The cylinders were removed and the F concentration of the solutions measured by ISE using TISAB decomplexant. F uptake was determined by difference from the original NaF concentration. The two conventional GICs showed reductions of 17.4 and 8.5% for ultrasound compared to standard set whereas the modified material increased by 32.3% and the experimental one by 20.6%. It is suggested that the effect of ultrasound may increase the surface area of the residual glass particles in the GIC which would increase F uptake. In GICs where considerable F ion is released into the cement matrix by the enhanced reaction caused by ultrasound this may be sufficient to reverse the former effect producing the reduced uptake observed.
超声已被证明可以改善玻璃离子水门汀(GIC)的性能,也可以改善其他水泥性能。特别是,氟化物的释放得到了增强。这些水泥还可以从液体中吸收氟离子。本研究旨在探讨超声对这种水泥性能的影响。使用了两种商业牙科修复 GIC 以及一种改良的商业材料和一种基于无氟玻璃的实验材料。所有三种商业材料都装在胶囊中,按制造商的指示混合,实验材料按以前的论文混合。混合的水泥被放置在聚乙烯模具中,以制成 3×2 毫米厚的圆盘。这些要么允许标准设置 6 分钟,要么用超声设置 55 秒。每种材料/设置制作了 18 个样本。三个样本被放置在 4ml 0.2%的 NaF 溶液中,在 37°C 下放置 24 小时。将圆柱体取出,用 TISAB 解络剂通过 ISE 测量溶液中的 F 浓度。F 摄取量通过与原始 NaF 浓度的差异来确定。与标准设置相比,两种传统 GIC 的超声吸收率分别降低了 17.4%和 8.5%,而改良材料增加了 32.3%,实验材料增加了 20.6%。有人认为,超声的作用可能会增加 GIC 中残留玻璃颗粒的表面积,从而增加 F 的吸收。在 GIC 中,由于超声增强反应释放出大量的氟离子到水泥基质中,这可能足以抵消先前观察到的吸收减少的影响。