Department of Prosthodontics, Karadeniz Technical University, Trabzon, Turkey.
J Adhes Dent. 2011 Dec;13(6):543-50. doi: 10.3290/j.jad.a19811.
To evaluate the influence of provisional luting cements on the bonding performance of a resin-based self-adhesive luting cement to dentin vs that of currently used resin-based luting agents with different adhesion strategies.
Forty-five prepared human molars were randomly and equally divided into three main groups according to the type of provisional luting cement applied: eugenol-containing provisional cement (Temp Bond, Kerr), eugenol-free provisional cement (Temp Bond NE, Kerr), and control where the provisionalization step was omitted. Each group was further subdivided into 3 groups based on the category of adhesive systems/ luting materials used: a two-step etch-and-rinse system (Single Bond/RelyX ARC; 3M ESPE) (RX), a two-step self-etching system (Clearfil Liner Bond 2V/ Panavia F; Kuraray) (PF), and a self-adhesive luting cement (Rely X Unicem; 3M ESPE) (RU). Finally, 9 groups of 5 teeth each were prepared for the microtensile test.
Two-way analysis of variance (ANOVA) and post-hoc Bonferroni tests revealed that definitive luting cement, provisional luting cement, and the interactions of these two factors had significant influences on dentin bond strength. The highest bond strength was obtained for PF (32.05 MPa), followed by RX (26.57 MPa) and RU (16.56 MPa) for the controls. Contamination with either eugenol-containing or eugenol-free provisional cement significantly decreased the bonding effectiveness of RX (19.08 and 19.69 MPa, respectively) and PF (14.21 and 16.67 MPa respectively) to dentin (p < 0.05). RU showed comparable bond strength values before and after provisional cement (13.93 and 14.49 MPa, respectively) application (p > 0.05). Eugenol in provisional luting cement did not produce material-related alterations in the bonding performance of the resin luting cements tested (p > 0.05).
Based on these results, the self-adhesive cement which was not influenced by the provisional cement application may be promising. However, long-term laboratory and clinical performance of this cement needs to be assessed before recommending it as an alternative to the technically more demanding approaches. Moreover, an effective surface cleansing procedure is critical to achieve a successful bond between the contaminated dentin and luting cement.
评估临时粘固剂对树脂基自粘结粘固剂与牙本质粘结性能的影响,与目前使用的具有不同粘结策略的树脂基粘固剂进行比较。
将 45 颗预备好的人磨牙随机平均分为三组,根据应用的临时粘固剂类型:含丁香酚的临时粘固剂(Temp Bond, Kerr)、无丁香酚的临时粘固剂(Temp Bond NE, Kerr)和省略临时粘固步骤的对照组。每组进一步根据粘结系统/粘固材料的类别分为 3 组:两步酸蚀-冲洗系统(Single Bond/RelyX ARC;3M ESPE)(RX)、两步自酸蚀系统(Clearfil Liner Bond 2V/Panavia F;Kuraray)(PF)和自粘结粘固剂(Rely X Unicem;3M ESPE)(RU)。最后,每组 5 颗牙共制备 9 组进行微拉伸试验。
双因素方差分析(ANOVA)和事后 Bonferroni 检验显示,最终粘固剂、临时粘固剂以及这两个因素的相互作用对牙本质粘结强度有显著影响。PF 组获得的粘结强度最高(32.05 MPa),其次是 RX 组(26.57 MPa)和 RU 组(16.56 MPa)对照组。无论是含丁香酚的临时粘固剂还是无丁香酚的临时粘固剂污染都会显著降低 RX(分别为 19.08 和 19.69 MPa)和 PF(分别为 14.21 和 16.67 MPa)对牙本质的粘结效果(p<0.05)。RU 组在应用临时粘固剂前后的粘结强度值相似(分别为 13.93 和 14.49 MPa)(p>0.05)。临时粘固剂中的丁香酚并没有改变所测试的树脂粘固剂的粘结性能(p>0.05)。
基于这些结果,不受临时粘固剂应用影响的自粘结粘固剂可能具有应用前景。然而,在推荐其作为技术要求更高的方法的替代方法之前,需要对这种粘固剂的长期实验室和临床性能进行评估。此外,有效的表面清洁程序对于实现污染牙本质和粘固剂之间的成功粘结至关重要。