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用于优化磁控溅射沉积薄膜实验参数的光谱诊断

[Spectrum diagnostics for optimization of experimental parameters in thin films deposited by magnetron sputtering].

作者信息

Guo Qing-Lin, Cui Yong-Liang, Chen Jian-Hui, Zhang Jin-Ping, Huai Su-Fang, Liu Bao-Ting, Chen Jin-Zhong

机构信息

College of Physics Science & Technology, Hebei University, Baoding 071002, China.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2010 Dec;30(12):3179-82.

Abstract

The plasma emission spectra generated during the deposition process of Si-based thin films by radio frequency (RF) magnetron sputtering using Cu and Al targets in an argon atmosphere were acquired by the plasma analysis system, which consists of a magnetron sputtering apparatus, an Omni-lambda300 series grating spectrometer, a CCD data acquisition system and an optical fiber transmission system. The variation in Cu and Al plasma emission spectra intensity depending on sputtering conditions, such as sputtering time, sputtering power, the target-to-substrate distance and deposition pressure, was studied by using the analysis lines Cu I 324. 754 nm, Cu I 327. 396 nm, Cu I 333. 784 nm, Cu I 353. 039 nm, Al I 394. 403 nm and Al I 396. 153 nm. Compared with the option of experimental parameters of thin films deposited by RF magnetron sputtering, it was shown that emission spectra analysis methods play a guiding role in optimizing the deposition conditions of thin films in RF magnetron sputtering.

摘要

通过由磁控溅射装置、Omni-lambda300系列光栅光谱仪、CCD数据采集系统和光纤传输系统组成的等离子体分析系统,获取了在氩气气氛中使用铜靶和铝靶通过射频(RF)磁控溅射沉积硅基薄膜过程中产生的等离子体发射光谱。利用分析谱线Cu I 324.754 nm、Cu I 327.396 nm、Cu I 333.784 nm、Cu I 353.039 nm、Al I 394.403 nm和Al I 396.153 nm,研究了铜和铝等离子体发射光谱强度随溅射条件(如溅射时间、溅射功率、靶材与衬底距离和沉积压力)的变化。与射频磁控溅射沉积薄膜的实验参数选择相比,结果表明发射光谱分析方法在优化射频磁控溅射薄膜的沉积条件方面具有指导作用。

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