Pourayoubi Mehrdad, Saneei Anahid
Department of Chemistry, Ferdowsi University of Mashhad, Mashhad 91779, Iran.
Acta Crystallogr Sect E Struct Rep Online. 2011 Feb 19;67(Pt 3):o665. doi: 10.1107/S1600536811005435.
In the title compound, C(8)H(17)ClF(2)N(3)O(2)P, the phosphoryl group and the NH unit of the C(O)NHP(O) moiety adopt a syn conformation with respect to each other. The P atom is in a tetra-hedral coordination environment and the environment of the N atom of the C(O)NHP(O) moiety is essentially planar. In the crystal, adjacent mol-ecules are linked via N-H⋯O =P and N-H⋯O =C hydrogen bonds, building R(2) (2)(8) and R(2) (2)(12) rings in a linear arrangement parallel to [110].
在标题化合物C(8)H(17)ClF(2)N(3)O(2)P中，磷酰基和C(O)NHP(O)部分的NH单元彼此呈顺式构象。P原子处于四面体配位环境，C(O)NHP(O)部分的N原子环境基本为平面。在晶体中，相邻分子通过N-H⋯O =P和N-H⋯O =C氢键相连，形成平行于[110]呈线性排列的R(2) (2)(8)和R(2) (2)(12)环。
