Ouzidan Younes, Kandri Rodi Youssef, Butcher Raymond J, Essassi El Mokhtar, El Ammari Lahcen
Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 8;67(Pt 2):o283. doi: 10.1107/S1600536810054164.
The crystal structure of the title compound, C(16)H(24)N(2)O, is built up from two fused six- and five-membered rings linked to C(9)H(19) chains. The fused-ring system is essentially planar, the largest deviation from the mean plane being 0.009 (2) Å. The chain is nearly perpendicular to this plane [dihedral angle = 80.27 (17)°]. In the crystal, inter-molecular N-H⋯O hydrogen bonds form dimers with an R(2) (2)(8) graph-set motif. These dimers are further connected through C-H⋯O hydrogen bonds, building sheets parallel to (100).
标题化合物C(16)H(24)N(2)O的晶体结构由两个稠合的六元环和五元环与C(9)H(19)链相连构成。稠环体系基本呈平面状，与平均平面的最大偏差为0.009 (2) Å。链几乎垂直于该平面[二面角 = 80.27 (17)°]。在晶体中，分子间N—H⋯O氢键形成具有R(2) (2)(8)图形集 motif的二聚体。这些二聚体通过C—H⋯O氢键进一步连接，形成平行于(100)的片层。
