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4-氨基-1-(2-苯甲酰基-1-苯基-乙基)-3-苯基-1H-1,2,4-三唑-5(4H)-硫酮

4-Amino-1-(2-benzoyl-1-phenyl-eth-yl)-3-phenyl-1H-1,2,4-triazol-5(4H)-thione.

作者信息

Song Xiao-Qiu, Ye Lin, Wang He-Wen

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 12;67(Pt 2):o347. doi: 10.1107/S1600536810054553.

DOI:10.1107/S1600536810054553
PMID:21523028
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3051625/
Abstract

In the title compound, C(23)H(20)N(4)OS, the two phenyl rings of the diphenyl-propanone fragment form a dihedral angle of 86.8 (1)°, and the third phenyl ring attached to the triazole ring is twisted from the latter at 40.1 (1)°. In the crystal, mol-ecules are paired into centrosymmetric dimers via pairs of inter-molecular N-H⋯O and N-H⋯S hydrogen bonds.

摘要

在标题化合物C₂₃H₂₀N₄OS中，二苯基丙酮片段的两个苯环形成86.8 (1)°的二面角，连接到三唑环上的第三个苯环与后者扭转40.1 (1)°。在晶体中，分子通过分子间N-H⋯O和N-H⋯S氢键对形成中心对称二聚体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a258/3051625/7077def63be9/e-67-0o347-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a258/3051625/7077def63be9/e-67-0o347-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a258/3051625/7077def63be9/e-67-0o347-fig1.jpg

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