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1-(2-溴乙基)-1,4-重氮双环-[2.2.2]辛烷溴化物磷酸二氢盐-磷酸(1/1)

1-(2-Bromo-ethyl)-1,4-diazo-niabicyclo-[2.2.2]octane bromide dihydrogen phosphate-phospho-ric acid (1/1).

作者信息

Xiao Jing-Mei

机构信息

Ordered Matter Science Research Center, College of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 May 15;66(Pt 6):o1339. doi: 10.1107/S1600536810017071.

DOI:10.1107/S1600536810017071
PMID:21579428
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2979413/
Abstract

In the crystal structure of the title compound, C(8)H(17)BrN(2) (2+)·Br(-)·H(2)PO(4) (-)·H(3)PO(4), the cations, anions and phospho-ric acid mol-ecules are linked by O-H⋯O, N-H⋯O and O-H⋯Br hydrogen bonds into layers parallel to (101).

摘要

在标题化合物C(8)H(17)BrN(2)(2+)·Br(-)·H(2)PO(4)(-)·H(3)PO(4)的晶体结构中，阳离子、阴离子和磷酸分子通过O-H⋯O、N-H⋯O和O-H⋯Br氢键连接成平行于(101)的层。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/989e/2979413/403c433c4341/e-66-o1339-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/989e/2979413/0f7d01d3af1a/e-66-o1339-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/989e/2979413/403c433c4341/e-66-o1339-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/989e/2979413/0f7d01d3af1a/e-66-o1339-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/989e/2979413/403c433c4341/e-66-o1339-fig2.jpg

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J Phys Chem B. 2008 Jun 5;112(22):6779-85. doi: 10.1021/jp801106m. Epub 2008 May 9.
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In situ hydrothermal synthesis of tetrazole coordination polymers with interesting physical properties.原位水热合成具有有趣物理性质的四唑配位聚合物。
Chem Soc Rev. 2008 Jan;37(1):84-100. doi: 10.1039/b616738c. Epub 2007 Oct 1.
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A short history of SHELX.
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Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.