1-（3-均三甲苯基-3-甲基-环丁基）-2-苯氧基-乙酮
1-(3-Mesityl-3-methyl-cyclo-butyl)-2-phenoxy-ethanone.
作者信息
Koca Murat, Kirilmiş Cumhur, Arici Cengiz
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2010 Feb 6;66(Pt 3):o523. doi: 10.1107/S1600536810003910.
Abstract
In the title compound, C(22)H(26)O(2), the cyclo-butane ring is puckered, with a dihedral angle of 24.97 (9)° between the two C(3) planes. In the crystal, inter-molecular non-classical C-H⋯O inter-actions between the methyl-cyclo-butyl CH group and the O atom of the phen-oxy group are found.
摘要
在标题化合物C₂₂H₂₆O₂中，环丁烷环呈皱折状，两个C(3)平面之间的二面角为24.97 (9)°。在晶体中，发现甲基环丁基的CH基团与苯氧基的O原子之间存在分子间非经典C-H⋯O相互作用。
相似文献
1
1-(3-Mesityl-3-methyl-cyclo-butyl)-2-phenoxy-ethanone.1-（3-均三甲苯基-3-甲基-环丁基）-2-苯氧基-乙酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Feb 6;66(Pt 3):o523. doi: 10.1107/S1600536810003910.
2
(Z)-1-(3-Mesityl-3-methyl-cyclo-but-yl)-2-(morpholin-4-yl)ethanone oxime.（Z）-1-（3-均三甲苯基-3-甲基-环丁基）-2-（吗啉-4-基）乙酮肟
Acta Crystallogr Sect E Struct Rep Online. 2011 Apr 1;67(Pt 4):o958-9. doi: 10.1107/S1600536811009408. Epub 2011 Mar 23.
3
2,2'-[(3-Bromo-4-hy-droxy-5-meth-oxy-phen-yl)methyl-idene]bis-(3-hy-droxy-5,5-dimethyl-cyclo-hex-2-en-1-one).2,2'-[(3-溴-4-羟基-5-甲氧基苯基)亚甲基]双-(3-羟基-5,5-二甲基环己-2-烯-1-酮)
Acta Crystallogr Sect E Struct Rep Online. 2012 Oct 1;68(Pt 10):o2875-6. doi: 10.1107/S1600536812037853. Epub 2012 Sep 8.
4
1-(4-Meth-oxy-phen-yl)-2-(1H-1,2,4-triazol-1-yl)ethanone.1-（4-甲氧基苯基）-2-（1H-1,2,4-三唑-1-基）乙酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Jul 10;66(Pt 8):o1978. doi: 10.1107/S160053681002653X.
5
Mesit-yl(2,4,6-trimeth-oxy-phen-yl)borinic acid.美西托（2,4,6-三甲氧基苯基）硼酸
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 18;66(Pt 7):o1711-2. doi: 10.1107/S160053681002297X.
6
Dihydro-allocryptopine.二氢别隐品碱
Acta Crystallogr Sect E Struct Rep Online. 2012 Jan;68(Pt 1):o69. doi: 10.1107/S1600536811052172. Epub 2011 Dec 10.
7
9-(4-Hy-droxy-3-meth-oxy-phen-yl)-3,3,6,6-tetra-methyl-3,4,5,6-tetra-hydro-9H-xanthene-1,8(2H,7H)-dione.9-(4-羟基-3-甲氧基苯基)-3,3,6,6-四甲基-3,4,5,6-四氢-9H-占吨-1,8(2H,7H)-二酮
Acta Crystallogr Sect E Struct Rep Online. 2010 Jun 5;66(Pt 7):o1538-9. doi: 10.1107/S1600536810020258.
8
12-(3,4,5-Tri-meth-oxy-phen-yl)-2,3,4,12-tetra-hydro-1H-5-oxa-tetra-phen-1-one: crystal structure and Hirshfeld surface analysis.12-(3,4,5-三甲氧基苯基)-2,3,4,12-四氢-1H-5-氧杂四苯-1-酮：晶体结构与 Hirshfeld 表面分析
Acta Crystallogr E Crystallogr Commun. 2016 May 13;72(Pt 6):809-14. doi: 10.1107/S2056989016007775. eCollection 2016 Jun 1.
9
Crystal structure of methyl 6-meth-oxy-11-(4-meth-oxy-phen-yl)-16-methyl-14-phenyl-8,12-dioxa-14,15-di-aza-tetra-cyclo-[8.7.0.0(2,7).0(13,17)]hepta-deca-2(7),3,5,13(17),15-penta-ene-10-carboxyl-ate.6-甲氧基-11-（4-甲氧基苯基）-16-甲基-14-苯基-8,12-二氧杂-14,15-二氮杂四环-[8.7.0.0(2,7).0(13,17)]十七碳-2(7),3,5,13(17),15-五烯-10-羧酸甲酯的晶体结构
Acta Crystallogr Sect E Struct Rep Online. 2014 Aug 9;70(Pt 9):127-9. doi: 10.1107/S1600536814017929. eCollection 2014 Sep 1.
10
Crystal structure of 2-meth-oxy-2-[(4-methyl-phen-yl)sulfan-yl]-1-phenyl-ethan-1-one.2-甲氧基-2-[(4-甲基苯基)硫烷基]-1-苯基乙-1-酮的晶体结构
Acta Crystallogr E Crystallogr Commun. 2015 Jan 1;71(Pt 1):o3-4. doi: 10.1107/S205698901402550X.
本文引用的文献
1
Structure validation in chemical crystallography.化学晶体学中的结构验证
Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
3
1-Methyl-1-phenyl-3-[1-hydroxyimino-2-(succinimido)ethyl]cyclobutane.1-甲基-1-苯基-3-[1-羟基亚氨基-2-(琥珀酰亚氨基)乙基]环丁烷
Acta Crystallogr C. 2004 Sep;60(Pt 9):o674-6. doi: 10.1107/S0108270104018074. Epub 2004 Aug 21.
4
Crystal structure of 4-(1-mesityl-1-methylcyclobutane-3-yl)-2-(N-ethyl)aminothiazole.
Anal Sci. 2002 Jun;18(6):725-6. doi: 10.2116/analsci.18.725.
5
Nonsteroidal antiinflammatory agents. 1.2,4-Diphenylthiazole-5-acetic acid and related compounds.非甾体抗炎药。1. 2,4-二苯基噻唑-5-乙酸及相关化合物。
J Med Chem. 1974 Nov;17(11):1177-81. doi: 10.1021/jm00257a010.
6
Antiparasitic 5-nitrothiazoles and 5-nitro-4-thiazolines. 4.抗寄生虫的5-硝基噻唑类和5-硝基-4-噻唑啉类。4.
J Med Chem. 1974 Feb;17(2):207-9. doi: 10.1021/jm00248a014.
7
Synthesis of antimicrobial agents. I. Synthesis and antimicrobial activities of thiazoloquinoline derivatives.抗菌剂的合成。I. 噻唑并喹啉衍生物的合成及抗菌活性
Chem Pharm Bull (Tokyo). 1979 Jan;27(1):1-11. doi: 10.1248/cpb.27.1.
Zotero 插件