Saeed Aamer, Khera Rasheed Ahmad, Abbas Naeem, Flörke Ulrich
Acta Crystallogr Sect E Struct Rep Online. 2008 Oct 25;64(Pt 11):o2209. doi: 10.1107/S1600536808034478.
In the title mol-ecule, C(13)H(16)FNO, the amide (N-C=O) plane is oriented at an angle of 29.9 (2)° with respect to the aromatic ring. The cyclo-hexane ring adopts the usual chair conformation. In the crystal structure, inter-molecular N-H⋯O hydrogen bonds link the mol-ecules into chains along [100]. A weak C-H⋯F inter-action is also observed. The F atom is disordered over two positions with occupancy factors of 0.873 (3) and 0.127 (3).
在标题分子C₁₃H₁₆FNO中,酰胺(N-C=O)平面相对于芳香环的取向角度为29.9(2)°。环己烷环呈常见的椅式构象。在晶体结构中,分子间的N-H⋯O氢键将分子沿[100]方向连接成链。还观察到一个弱的C-H⋯F相互作用。F原子在两个位置上无序分布,占据因子分别为0.873(3)和0.127(3)。