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双[4-(二甲基氨基)吡啶鎓]六[溴化物/氯化物(0.78/0.22)]锡(IV)酸盐

Bis[4-(dimethyl-amino)pyridinium] hexa-kis[bromido/chlorido(0.78/0.22)]stannate(IV).

作者信息

Lo Kong Mun, Ng Seik Weng

机构信息

Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 6;65(Pt 7):m715. doi: 10.1107/S1600536809019734.

DOI:10.1107/S1600536809019734
PMID:21582659
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2969252/
Abstract

The Sn atom in the title salt, (C(7)H(11)N(2))(2)[SnBr(4.67)Cl(1.33)], lies on a center of symmetry within an octa-hedron of disordered halogen atoms. The three independent halogen atoms are each a mixture of bromine and chlorine atoms [with site occupancies for bromine of 0.614 (1), 0.831 (1) and 0.888 (1)]. An N-H⋯ hydrogen bond is present.

摘要

在标题盐（C₇H₁₁N₂）₂[SnBr₄.₆₇Cl₁.₃₃]中，Sn原子位于由无序卤素原子构成的八面体的对称中心上。三个独立的卤素原子各自都是溴原子和氯原子的混合物[溴的位点占有率分别为0.614（1）、0.831（1）和0.888（1）]。存在一个N - H⋯氢键。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2d0e/2969252/848d95effcc4/e-65-0m715-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2d0e/2969252/848d95effcc4/e-65-0m715-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2d0e/2969252/848d95effcc4/e-65-0m715-fig1.jpg

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本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2009 May 14;65(Pt 6):m645. doi: 10.1107/S160053680901705X.
2
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Acta Crystallogr Sect E Struct Rep Online. 2008 May 21;64(Pt 6):m834. doi: 10.1107/S1600536808014669.
3
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.