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3-溴-9-(4-氯苄基)-9H-咔唑

3-Bromo-9-(4-chloro-benz-yl)-9H-carbazole.

作者信息

Xiao Zi-Dan, Pan Tong, Yang Dao-Wu

机构信息

College of Chemistry and Bioengineering, Changsha University of Science and Technology, Changsha 410076, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 6;65(Pt 7):o1476. doi: 10.1107/S1600536809019448.

DOI:10.1107/S1600536809019448
PMID:21582778
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2969400/
Abstract

The title compound, C(19)H(13)BrClN, was synthesized by N-alkyl-ation of 4-chloro-1-(chloro-meth-yl)benzene with 3-bromo-9H-carbazole. The carbazole ring system is essentially planar, with a mean deviation of 0.028 Å, and it makes a dihedral angle of 91.2 (3) Å with the plane of the benzene ring.

摘要

标题化合物C(19)H(13)BrClN是通过4-氯-1-(氯甲基)苯与3-溴-9H-咔唑的N-烷基化反应合成的。咔唑环系基本呈平面状，平均偏差为0.028 Å，且它与苯环平面形成的二面角为91.2 (3) Å。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3c79/2969400/b33f4765b839/e-65-o1476-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3c79/2969400/b33f4765b839/e-65-o1476-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3c79/2969400/b33f4765b839/e-65-o1476-fig1.jpg

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本文引用的文献

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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.