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3-溴-9-(4-氟苄基)-9H-咔唑

3-Bromo-9-(4-fluoro-benz-yl)-9H-carbazole.

作者信息

Wang Cheng-Feng

机构信息

College of Chemistry & Bioengineering, Changsha University of Science & Technology, Changsha 410076, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 17;65(Pt 7):o1589. doi: 10.1107/S160053680901976X.

DOI:10.1107/S160053680901976X
PMID:21582864
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2969443/
Abstract

The title compound, C(19)H(13)BrFN, was synthesized by N-alkyl-ation of 1-chloro-methyl-4-fluoro-benzene with 3-bromo-9H-carbazole. The carbazole ring system is essentially planar (r.m.s. deviation of 0.024 Å for the non-H atoms) and forms a dihedral angle of 88.2 (3)° with the benzene ring.

摘要

标题化合物C(19)H(13)BrFN是通过1-氯甲基-4-氟苯与3-溴-9H-咔唑的N-烷基化反应合成的。咔唑环体系基本呈平面状（非H原子的均方根偏差为0.024 Å），与苯环形成88.2 (3)°的二面角。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d5ac/2969443/901bde72b91d/e-65-o1589-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d5ac/2969443/901bde72b91d/e-65-o1589-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d5ac/2969443/901bde72b91d/e-65-o1589-fig1.jpg

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本文引用的文献

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