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Di-μ-sulfato-κO:O'-bis-[diaqua-(1H-imidazo[4,5-f][1,10]phenanthroline-κN,N)cobalt(II)] dihydrate.

作者信息

Gong Yun, Zhou Yuchao, Li Jinghua, Wu Xiaoxia, Qin Jianbo

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 1;65(Pt 8):m844-5. doi: 10.1107/S1600536809024295.

DOI:10.1107/S1600536809024295
PMID:21583315
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977338/
Abstract

In the centrosymmetric dinuclear title compound, [Co(2)(SO(4))(2)(C(13)H(8)N(4))(2)(H(2)O)(4)]·2H(2)O, the Co(II) atom is coord-in-ated by two N atoms from two 1H-imidazo[4,5-f][1,10]phenanthroline ligands, two O atoms from two sulfate anions and two O atoms from water mol-ecules in a distorted octa-hedral geometry. The Co⋯Co separation is 5.1167 (7) Å. The coordinated and uncoordinated water mol-ecules engage in N-H⋯O and O-H⋯O hydrogen-bonding inter-actions.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/05bc/2977338/9656a8491889/e-65-0m844-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/05bc/2977338/fb3defdc57b1/e-65-0m844-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/05bc/2977338/9656a8491889/e-65-0m844-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/05bc/2977338/fb3defdc57b1/e-65-0m844-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/05bc/2977338/9656a8491889/e-65-0m844-fig2.jpg

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引用本文的文献

1
Di-μ-sulfato-κO:O'-bis-[diaqua-(1H-imidazo[4,5-f][1,10]phenanthroline)manganese(II)] dihydrate.
Acta Crystallogr Sect E Struct Rep Online. 2010 Aug 18;66(Pt 9):m1115-6. doi: 10.1107/S1600536810031909.

本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
2
[Ruthenium(II)(bpy)(2)L](2+), where L are imidazo[f]-1,10-phenanthrolines: synthesis, photophysics and binding with DNA.[钌（II）（联吡啶）₂L]²⁺，其中L为咪唑并[f]-1,10-菲咯啉：合成、光物理性质及与DNA的结合
Spectrochim Acta A Mol Biomol Spectrosc. 2004 Sep;60(11):2635-41. doi: 10.1016/j.saa.2004.01.002.