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3-（4-氯-苯基-磺酰基）-8-甲基-1,3-二氮杂螺[4.5]癸烷-2,4-二酮

3-(4-Chloro-phenyl-sulfon-yl)-8-methyl-1,3-diaza-spiro-[4.5]decane-2,4-dione.

作者信息

Kashif M Kalim, Khawar Rauf M, Bolte Michael, Hameed Shahid

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 18;65(Pt 8):o1893. doi: 10.1107/S1600536809027482.

DOI:10.1107/S1600536809027482
PMID:21583583
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977302/
Abstract

In the title compound, C(15)H(17)ClN(2)O(4)S, the atoms in the hydantoin ring are coplanar (r.m.s. deviation = 0.006 Å). The crystal structure is stabilized by inter-molecular N-H⋯O hydrogen bonds which link the mol-ecules into centrosymmetric dimers. The dihedral angle subtended by the 4-chloro-phenyl group with the plane passing through the hydantoin unit is 82.98 (4)°. The cyclo-hexyl ring adopts an ideal chair conformation.

摘要

在标题化合物C(15)H(17)ClN(2)O(4)S中，乙内酰脲环中的原子是共面的（均方根偏差 = 0.006 Å）。晶体结构通过分子间N-H⋯O氢键得以稳定，这些氢键将分子连接成中心对称的二聚体。4-氯苯基与通过乙内酰脲单元的平面所形成的二面角为82.98 (4)°。环己基环呈理想的椅式构象。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/07b5/2977302/7156e5a0516d/e-65-o1893-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/07b5/2977302/a8dc5c5efffa/e-65-o1893-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/07b5/2977302/7156e5a0516d/e-65-o1893-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/07b5/2977302/a8dc5c5efffa/e-65-o1893-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/07b5/2977302/7156e5a0516d/e-65-o1893-fig2.jpg

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