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2,2'-二氯-1,1'-[(戊烷-1,5-二氧基)双-(亚氨基甲基亚基)]二苯

2,2'-Dichloro-1,1'-[(pentane-1,5-diyldi-oxy)bis-(nitrilo-methyl-idyne)]dibenzene.

作者信息

Dong Wen-Kui, Tong Jun-Feng, Wu Jian-Chao, Li Li, Yao Jian

机构信息

School of Chemical and Biological Engineering, Lanzhou Jiaotong University, Lanzhou 730070, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 18;65(Pt 8):o1904. doi: 10.1107/S1600536809027433.

DOI:10.1107/S1600536809027433
PMID:21583594
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977418/
Abstract

The mol-ecule of the title compound, C(19)H(20)Cl(2)N(2)O(2), which lies across a crystallographic inversion centre, adopts a linear configuration. The dihedral angle between the two halves of the mol-ecule is 5.14 (2)°. In the crystal structure, inter-molecular C-H⋯O hydrogen bonds link neighbouring mol-ecules into an infinite zigzag chain supra-molecular structure.

摘要

标题化合物C(19)H(20)Cl(2)N(2)O(2)的分子位于一个晶体学反演中心上，呈线性构型。分子两半部分之间的二面角为5.14 (2)°。在晶体结构中，分子间的C—H⋯O氢键将相邻分子连接成无限之字形链超分子结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0871/2977418/8f51395500cb/e-65-o1904-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0871/2977418/78a1fb703105/e-65-o1904-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0871/2977418/8f51395500cb/e-65-o1904-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0871/2977418/78a1fb703105/e-65-o1904-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0871/2977418/8f51395500cb/e-65-o1904-fig2.jpg

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本文引用的文献

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2,2'-{1,1'-[Butane-1,4-diyl-bis(oxy-nitrilo)]di-ethylidyne}di-1-naphthol.2,2'-{1,1'-[丁烷-1,4-二基-双(氧基腈)]二亚乙基}二-1-萘酚。
Acta Crystallogr Sect E Struct Rep Online. 2009 May 14;65(Pt 6):o1248. doi: 10.1107/S160053680901647X.
2
2,2'-{1,1'-[Pentane-1,5-diylbis(oxy-nitrilo)]diethylidyne}di-1-naphthol.2,2'-{1,1'-[戊烷-1,5-二基双(氧代腈基)]二亚乙基}二-1-萘酚。
Acta Crystallogr Sect E Struct Rep Online. 2009 May 14;65(Pt 6):o1238. doi: 10.1107/S1600536809016584.
3
6,6'-Dihydr-oxy-2,2'-[(pentane-1,5-diyl-dioxy)bis-(nitrilo-methyl-idyne)]diphenol.
6,6'-二羟基-2,2'-[(戊烷-1,5-二基二氧基)双(亚氨甲基亚基)]二苯酚。
Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 26;64(Pt 8):o1600-1. doi: 10.1107/S1600536808023064.
4
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.