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4-（4-氰基-2-氟苯氧基）苯基 4-甲基苯磺酸盐

4-(4-Cyano-2-fluoro-phen-oxy)phenyl 4-methyl-benzene-sulfonate.

作者信息

Luo Shuping, Zhang Jixu, Wang Jianfeng, Li Bailin

机构信息

State Key Laboratory Breeding Base of Green Chemistry-Synthesis Technology, Zhejiang University of Technology, Hangzhou 310014, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 29;65(Pt 8):o2011. doi: 10.1107/S1600536809029201.

DOI:10.1107/S1600536809029201
PMID:21583682
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977414/
Abstract

The title compound, C(20)H(14)FNO(4)S, was synthesized from hydro-quinone, p-toluene-sulfonyl chloride and 3,4-difluoro-benzonitrile. A folded conformation is adopted by the crystal structure. Inter-molecular C-H⋯N hydrogen bonds form dimers arranged around inversion centers.

摘要

标题化合物C(20)H(14)FNO(4)S由对苯二酚、对甲苯磺酰氯和3,4-二氟苯腈合成。晶体结构采用折叠构象。分子间C-H⋯N氢键形成围绕对称中心排列的二聚体。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d30/2977414/5bb27f1587db/e-65-o2011-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d30/2977414/c9e2b0756e3f/e-65-o2011-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d30/2977414/5bb27f1587db/e-65-o2011-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d30/2977414/c9e2b0756e3f/e-65-o2011-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1d30/2977414/5bb27f1587db/e-65-o2011-fig2.jpg

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