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[5-(2,4-二氯苯基)-1,3,4-噻二唑-2-基氨基](4-甲氧基苯基)甲基膦酸二乙酯

Diethyl {[5-(2,4-dichloro-phen-yl)-1,3,4-thia-diazol-2-ylamino](4-methoxy-phenyl)methyl}-phospho-nate.

作者信息

Wang Yao, Wan Rong, Yin Li-He, Han Feng, Wang Peng

机构信息

Department of Applied Chemistry, College of Science, Nanjing University of Technology, No.5 Xinmofan Road, Nanjing, Nanjing 210009, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Apr 8;65(Pt 5):o983. doi: 10.1107/S1600536809012471.

DOI:10.1107/S1600536809012471
PMID:21584021
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2977678/
Abstract

The title compound, C(20)H(22)Cl(2)N(3)O(4)PS, was synthesized by the reaction of N-(4-methoxy-benzyl-idene)-5-(2,4-dichloro-phenyl)-1,3,4-thia-diazol-2-amine and diethyl phosphite. In the crystal, inter-molecular C-H⋯O and N-H⋯O hydrogen bonds link the mol-ecules.

摘要

标题化合物C(20)H(22)Cl(2)N(3)O(4)PS是由N-(4-甲氧基-亚苄基)-5-(2,4-二氯苯基)-1,3,4-噻二唑-2-胺与亚磷酸二乙酯反应合成的。在晶体中，分子间的C-H⋯O和N-H⋯O氢键将分子连接起来。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb4/2977678/9154732a8c69/e-65-0o983-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb4/2977678/f65f890f02a6/e-65-0o983-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb4/2977678/9154732a8c69/e-65-0o983-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb4/2977678/f65f890f02a6/e-65-0o983-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1fb4/2977678/9154732a8c69/e-65-0o983-fig2.jpg

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本文引用的文献

1
Diethyl {(4-methoxy-phen-yl)[5-(4-nitro-phen-yl)-1,3,4-thia-diazol-2-ylamino]meth-yl}phospho-nate.二乙基{(4-甲氧基-苯基)[5-(4-硝基-苯基)-1,3,4-噻二唑-2-基氨基]甲基}膦酸酯
Acta Crystallogr Sect E Struct Rep Online. 2008 Jul 5;64(Pt 8):o1376. doi: 10.1107/S1600536808017364.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.