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Poly[(μ(4)-biphenyl-3,3'-dicarboxyl-ato)bis[μ(2)-1,1'-(butane-1,4-di-yl)diimidazole](μ(2)-oxalato)dimanganese(II)].

作者信息

Zhu Bao-Yong

机构信息

Department of Chemistry, Dezhou University, Dezhou Shandong 253023, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 4;66(Pt 10):m1214. doi: 10.1107/S1600536810035269.

DOI:10.1107/S1600536810035269
PMID:21587372
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2983367/
Abstract

In the title coordination compound, Mn(2)(C(14)H(8)O(4))(C(2)O(4))(C(10)H(14)N(4))(2), the biphenyl-3,3'-dicarboxyl-ate and oxalate anions, both situated on inversion centres, function in a bridging mode, linking the dinuclear Mn(II) atoms into wave-like layers. Each 1,1'-(1,4-butane-1,4-di-yl)diimidazole ligand coordinates to two Mn(II) atoms located in adjacent layers via Mn-N coordination bonds, giving a three-dimensional network. As the methyl-ene groups can bend freely relative to each other due to the C atoms connected via single bonds, the 1,1'-(butane-1,4-di-yl)diimidazole ligand forms an S-shaped conformation, which makes the void in the three-dimensional network distorted.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/36f72496b0cf/e-66-m1214-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/b055b9d810bb/e-66-m1214-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/7179fba7643a/e-66-m1214-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/36f72496b0cf/e-66-m1214-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/b055b9d810bb/e-66-m1214-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/7179fba7643a/e-66-m1214-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/cd54/2983367/36f72496b0cf/e-66-m1214-fig3.jpg

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