Feng Hai, Xing Bin Tao, Huang Xin, Zhou Ya Jian, Song Ying
College of Pharmaceutical Sciences, Zhejiang University of Technology, Hangzhou 310014, People's Republic of China.
Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 25;66(Pt 10):o2605. doi: 10.1107/S1600536810033878.
The title compound, C(11)H(17)ClNO(+)·C(8)H(7)O(2) (-), was obtained by the reaction of chlorprenaline {or 1-(2-chloro-phen-yl)-2-[(1-methyl-eth-yl)amino]-ethanol} and p-toluic acid. The chlorpren-aline is twisted moderately with a C-C-C-C torsion angle of 109.6 (2)°. The two mol-ecules are linked by classical O-H⋯O and N-H⋯O hydrogen bonds. Further N-H⋯O hydrogen bonds link two of these units into dimers.
标题化合物C(11)H(17)ClNO(+)·C(8)H(7)O(2) (-) 是通过氯丙那林 {即1-(2-氯苯基)-2-[(1-甲基乙基)氨基]乙醇} 与对甲苯甲酸反应得到的。氯丙那林以109.6 (2)°的C-C-C-C扭转角适度扭转。两个分子通过经典的O-H⋯O和N-H⋯O氢键相连。进一步的N-H⋯O氢键将其中两个单元连接成二聚体。
